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(ZE,E)-3-dimethylpent-1,3-dienyl phenyl sulphone

Base Information Edit
  • Chemical Name:(ZE,E)-3-dimethylpent-1,3-dienyl phenyl sulphone
  • CAS No.:100289-52-9
  • Molecular Formula:C12H14O2S
  • Molecular Weight:222.308
  • Hs Code.:
  • Mol file:100289-52-9.mol
(ZE,E)-3-dimethylpent-1,3-dienyl phenyl sulphone

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Chemical Property of (ZE,E)-3-dimethylpent-1,3-dienyl phenyl sulphone Edit
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Technology Process of (ZE,E)-3-dimethylpent-1,3-dienyl phenyl sulphone

There total 3 articles about (ZE,E)-3-dimethylpent-1,3-dienyl phenyl sulphone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 3 steps
1: 1.) butyl-lithium, N,N,N',N'-tetramethyl-ethylenediamine / 1.) THF, -40 deg C, 1 h 2.) THF, -60 deg C, 30 min then warming to room temp. during 12 h
2: 96 percent / peracetic acid / CH2Cl2 / 1.) 0 deg C, 90 min 2.) 16 h, room temp.
3: 1.) butyl lithium / 1.) DME, -78 deg C, hexane, 20 min 2.) neat or DME, room temp.
With peracetic acid; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In dichloromethane;
Guidance literature:
Multi-step reaction with 2 steps
1: 96 percent / peracetic acid / CH2Cl2 / 1.) 0 deg C, 90 min 2.) 16 h, room temp.
2: 1.) butyl lithium / 1.) DME, -78 deg C, hexane, 20 min 2.) neat or DME, room temp.
With peracetic acid; n-butyllithium; In dichloromethane;
Guidance literature:
With n-butyllithium; Yield given. Multistep reaction; 1.) DME, -78 deg C, hexane, 20 min 2.) neat or DME, room temp.;
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