Technology Process of C16H26N2O4
There total 5 articles about C16H26N2O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
di-tert-butyl dicarbonate; C11H16N4O2;
With
palladium on activated charcoal; hydrogen;
In
ethanol;
at 20 ℃;
With
pyridine; hydroxylamine hydrochloride;
at 80 ℃;
for 2h;
With
hydrogenchloride; palladium on activated charcoal; hydrogen;
In
ethanol; water;
at 20 ℃;
for 15h;
DOI:10.1016/j.bmcl.2012.06.059
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium azide; tetrabutylammomium bromide; potassium iodide / toluene / Reflux
2.1: palladium on activated charcoal; hydrogen / ethanol / 20 °C
2.2: 2 h / 80 °C
2.3: 15 h / 20 °C
With
sodium azide; palladium on activated charcoal; tetrabutylammomium bromide; hydrogen; potassium iodide;
In
ethanol; toluene;
DOI:10.1016/j.bmcl.2012.06.059
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogenchloride; palladium on activated charcoal / methanol; water / 15 h / 20 °C
2.1: potassium carbonate / acetone / 3 h / Reflux
3.1: sodium azide; tetrabutylammomium bromide; potassium iodide / toluene / Reflux
4.1: palladium on activated charcoal; hydrogen / ethanol / 20 °C
4.2: 2 h / 80 °C
4.3: 15 h / 20 °C
With
hydrogenchloride; sodium azide; palladium on activated charcoal; tetrabutylammomium bromide; hydrogen; potassium carbonate; potassium iodide;
In
methanol; ethanol; water; acetone; toluene;
DOI:10.1016/j.bmcl.2012.06.059
