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C16H26N2O4

Base Information Edit
C<sub>16</sub>H<sub>26</sub>N<sub>2</sub>O<sub>4</sub>

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Suppliers and Price of C16H26N2O4
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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of C16H26N2O4 Edit
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Technology Process of C16H26N2O4

There total 5 articles about C16H26N2O4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
di-tert-butyl dicarbonate; C11H16N4O2; With palladium on activated charcoal; hydrogen; In ethanol; at 20 ℃;
With pyridine; hydroxylamine hydrochloride; at 80 ℃; for 2h;
With hydrogenchloride; palladium on activated charcoal; hydrogen; In ethanol; water; at 20 ℃; for 15h;
DOI:10.1016/j.bmcl.2012.06.059
Guidance literature:
Multi-step reaction with 2 steps
1.1: sodium azide; tetrabutylammomium bromide; potassium iodide / toluene / Reflux
2.1: palladium on activated charcoal; hydrogen / ethanol / 20 °C
2.2: 2 h / 80 °C
2.3: 15 h / 20 °C
With sodium azide; palladium on activated charcoal; tetrabutylammomium bromide; hydrogen; potassium iodide; In ethanol; toluene;
DOI:10.1016/j.bmcl.2012.06.059
Guidance literature:
Multi-step reaction with 4 steps
1.1: hydrogenchloride; palladium on activated charcoal / methanol; water / 15 h / 20 °C
2.1: potassium carbonate / acetone / 3 h / Reflux
3.1: sodium azide; tetrabutylammomium bromide; potassium iodide / toluene / Reflux
4.1: palladium on activated charcoal; hydrogen / ethanol / 20 °C
4.2: 2 h / 80 °C
4.3: 15 h / 20 °C
With hydrogenchloride; sodium azide; palladium on activated charcoal; tetrabutylammomium bromide; hydrogen; potassium carbonate; potassium iodide; In methanol; ethanol; water; acetone; toluene;
DOI:10.1016/j.bmcl.2012.06.059
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