(1,6-Anhydro-3-desoxy-β-D-altropyranos-3-yl)bis<3-<(3,6-didesoxy-3-(2,4-dinitroanilino)-1,2-O-isopropyliden-α-D-glucofuranos-6-yl)amino>-3,6-didesoxy-1,2-O-isopropyliden-α-D-glucofuranos-6-yl>amin

Base Information

Chemical Name:(1,6-Anhydro-3-desoxy-β-D-altropyranos-3-yl)bis<3-<(3,6-didesoxy-3-(2,4-dinitroanilino)-1,2-O-isopropyliden-α-D-glucofuranos-6-yl)amino>-3,6-didesoxy-1,2-O-isopropyliden-α-D-glucofuranos-6-yl>amin
CAS No.:80970-88-3
Molecular Formula:C₅₄H₇₅N₉O₂₈
Molecular Weight:1298.23
Hs Code.:

(1,6-Anhydro-3-desoxy-β-D-altropyranos-3-yl)bis<3-<(3,6-didesoxy-3-(2,4-dinitroanilino)-1,2-O-isopropyliden-α-D-glucofuranos-6-yl)amino>-3,6-didesoxy-1,2-O-isopropyliden-α-D-glucofuranos-6-yl>amin

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Chemical Property of (1,6-Anhydro-3-desoxy-β-D-altropyranos-3-yl)bis<3-<(3,6-didesoxy-3-(2,4-dinitroanilino)-1,2-O-isopropyliden-α-D-glucofuranos-6-yl)amino>-3,6-didesoxy-1,2-O-isopropyliden-α-D-glucofuranos-6-yl>amin

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Technology Process of (1,6-Anhydro-3-desoxy-β-D-altropyranos-3-yl)bis<3-<(3,6-didesoxy-3-(2,4-dinitroanilino)-1,2-O-isopropyliden-α-D-glucofuranos-6-yl)amino>-3,6-didesoxy-1,2-O-isopropyliden-α-D-glucofuranos-6-yl>amin

There total 10 articles about (1,6-Anhydro-3-desoxy-β-D-altropyranos-3-yl)bis<3-<(3,6-didesoxy-3-(2,4-dinitroanilino)-1,2-O-isopropyliden-α-D-glucofuranos-6-yl)amino>-3,6-didesoxy-1,2-O-isopropyliden-α-D-glucofuranos-6-yl>amin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 70-34-8,65727-75-5
2,4-Dinitrofluorobenzene

: 80970-87-2
C₄₂H₇₁N₅O₂₀

: 80970-88-3
(1,6-Anhydro-3-desoxy-β-D-altropyranos-3-yl)bis<3-<(3,6-didesoxy-3-(2,4-dinitroanilino)-1,2-O-isopropyliden-α-D-glucofuranos-6-yl)amino>-3,6-didesoxy-1,2-O-isopropyliden-α-D-glucofuranos-6-yl>amin

Guidance literature:: With sodium hydrogencarbonate; In ethanol; water; for 12h;

Reference yield:

: 35905-31-8
Benzyl 2,3-anhydro-4,6-O-benzylidene-α-D-mannopyranoside

: 80970-88-3
(1,6-Anhydro-3-desoxy-β-D-altropyranos-3-yl)bis<3-<(3,6-didesoxy-3-(2,4-dinitroanilino)-1,2-O-isopropyliden-α-D-glucofuranos-6-yl)amino>-3,6-didesoxy-1,2-O-isopropyliden-α-D-glucofuranos-6-yl>amin

Guidance literature:: Multi-step reaction with 10 steps

1: 78 percent / NaN₃, NH₄Cl / 2-methoxy-ethanol; H₂O / 4 h / Heating

2: H₂ / 10percent Pd/C / methanol / 2 h

3: 0.5N HCl / H₂O / 10 h / Heating

4: 110 mg / Amberlite IRA 400 OH(-) / methanol; H₂O

5: 49 percent / methanol / 4 h / Heating

6: 81 percent / 2-methoxy-ethanol / 8 h / Heating

7: 0.43 mmol / H₂ / 10percent Pd/C / methanol / 2 h

8: 56 percent / ethanol / 4 h / Heating

9: 0.32 mmol / H₂ / 10percent Pd/C / 2 h

10: 57 percent / NaHCO₃ / ethanol; H₂O / 12 h

With hydrogenchloride; sodium azide; Amberlite IRA 400 OH(-); hydrogen; sodium hydrogencarbonate; ammonium chloride; palladium on activated charcoal; In methanol; ethanol; 2-methoxy-ethanol; water;

Reference yield:

: 80970-55-4
3-amino-1,6-anhydro-3-deoxy-β-D-altropyranose

: 80970-88-3
(1,6-Anhydro-3-desoxy-β-D-altropyranos-3-yl)bis<3-<(3,6-didesoxy-3-(2,4-dinitroanilino)-1,2-O-isopropyliden-α-D-glucofuranos-6-yl)amino>-3,6-didesoxy-1,2-O-isopropyliden-α-D-glucofuranos-6-yl>amin

Guidance literature:: Multi-step reaction with 6 steps

1: 49 percent / methanol / 4 h / Heating

2: 81 percent / 2-methoxy-ethanol / 8 h / Heating

3: 0.43 mmol / H₂ / 10percent Pd/C / methanol / 2 h

4: 56 percent / ethanol / 4 h / Heating

5: 0.32 mmol / H₂ / 10percent Pd/C / 2 h

6: 57 percent / NaHCO₃ / ethanol; H₂O / 12 h

With hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In methanol; ethanol; 2-methoxy-ethanol; water;