phosphinodithioic acid trimethylsilylester

Base Information

Chemical Name:phosphinodithioic acid trimethylsilylester
CAS No.:56152-29-5
Molecular Formula:C₁₅H₁₉PS₂Si
Molecular Weight:322.507
Hs Code.:

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Chemical Property of phosphinodithioic acid trimethylsilylester

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Technology Process of phosphinodithioic acid trimethylsilylester

There total 1 articles about phosphinodithioic acid trimethylsilylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 56152-29-5
phosphinodithioic acid trimethylsilylester

Guidance literature:: (C6H5)2P(S)SNa, ClSi(CH3)3;
DOI:10.1002/zaac.19754130307

Reference yield: 60.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 56152-29-5
phosphinodithioic acid trimethylsilylester

: 7773-01-5
manganese(ll) chloride

: 919772-98-8
[Mn(diphenyldithiophosphinato)2(tetrahydrofuran)2]

Guidance literature:: With P(CH₂CH₂CH₃)3; In tetrahydrofuran; under N2; P(n-Pr)3 added to suspn. of Mn salt in THF at room temp., Ph2PS(SSiMe3) added dropwise under stirring, mixt. stirred for 2 h; concd., recrystd. under warming;
DOI:10.1002/zaac.200600023

Reference yield: 38.0%

: 56152-29-5
phosphinodithioic acid trimethylsilylester

: 2966-50-9
silver trifluoroacetate

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: [Ag(Ph₂PS₂)(1,2-bis(diphenylphosphino)ethane)].infin.

Guidance literature:: In dichloromethane; under N2 atm. to soln. CF3COOAg and dppe in CH2Cl2 at -40°C Ph2P(S)SSiMe3 was added, stirred at -40°C and allowed to warm to room temp.; soln. was filtered and concd., hexane was added, 1 day at room temp.; elem. anal.;
DOI:10.1039/b501360g