7-(4-chlorobenzyl)-6-(4-fluorophenyl)-2-isopropyl-4-methyl-5-(4-methylbenzylidene)-6,7-dihydro-5H-pyrrolo[2,3-d]pyrimidine-6-carboxylic acid 4-chlorobenzylamide

Base Information

• Chemical Name: 7-(4-chlorobenzyl)-6-(4-fluorophenyl)-2-isopropyl-4-methyl-5-(4-methylbenzylidene)-6,7-dihydro-5H-pyrrolo[2,3-d]pyrimidine-6-carboxylic acid 4-chlorobenzylamide
• CAS No.: 1236283-20-7
• Molecular Formula: C₃₉H₃₅Cl₂FN₄O
• Molecular Weight: 665.638

Synonyms:

Chemical Property of 7-(4-chlorobenzyl)-6-(4-fluorophenyl)-2-isopropyl-4-methyl-5-(4-methylbenzylidene)-6,7-dihydro-5H-pyrrolo[2,3-d]pyrimidine-6-carboxylic acid 4-chlorobenzylamide

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Technology Process of 7-(4-chlorobenzyl)-6-(4-fluorophenyl)-2-isopropyl-4-methyl-5-(4-methylbenzylidene)-6,7-dihydro-5H-pyrrolo[2,3-d]pyrimidine-6-carboxylic acid 4-chlorobenzylamide

There total 2 articles about 7-(4-chlorobenzyl)-6-(4-fluorophenyl)-2-isopropyl-4-methyl-5-(4-methylbenzylidene)-6,7-dihydro-5H-pyrrolo[2,3-d]pyrimidine-6-carboxylic acid 4-chlorobenzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

N-(4-chlorobenzyl)-2-[(4-chlorobenzyl)-(2-isopropyl-6-methyl-5-ptolylethynylpyrimidin-4-yl)-amino]-2-(4-fluorophenyl)-acetamide (1236282-94-2) → 7-(4-chlorobenzyl)-6-(4-fluorophenyl)-2-isopropyl-4-methyl-5-(4-methylbenzylidene)-6,7-dihydro-5H-pyrrolo[2,3-d]pyrimidine-6-carboxylic acid 4-chlorobenzylamide (1236283-20-7)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol;

DOI:10.1021/jo100759b

Reference yield: 75.0%

N-(4-chlorobenzyl)-2-[(4-chlorobenzyl)-(2-isopropyl-6-methyl-5-ptolylethynylpyrimidin-4-yl)-amino]-2-(4-fluorophenyl)-acetamide (1236282-94-2) → 7-(4-chlorobenzyl)-6-(4-fluorophenyl)-2-isopropyl-4-methyl-5-(4-methylbenzylidene)-6,7-dihydro-5H-pyrrolo[2,3-d]pyrimidine-6-carboxylic acid 4-chlorobenzylamide (1236283-20-7) + 7-(4-chlorobenzyl)-6-(4-fluorophenyl)-2-isopropyl-4-methyl-5-(4-methylbenzylidene)-6,7-dihydro-5H-pyrrolo[2,3-d]pyrimidine-6-carboxylic acid 4-chlorobenzylamide (1236283-22-9)

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran; optical yield given as %de;

DOI:10.1021/jo100759b

upstream raw materials:

N-(4-chlorobenzyl)-2-[(4-chlorobenzyl)-(2-isopropyl-6-methyl-5-ptolylethynylpyrimidin-4-yl)-amino]-2-(4-fluorophenyl)-acetamide

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