trans-(PPh₃)2Pd(C₆H₄-4-SC(O)Me)(I)

Base Information

Chemical Name:trans-(PPh₃)2Pd(C₆H₄-4-SC(O)Me)(I)
CAS No.:886970-58-7
Molecular Formula:C₄₄H₃₇IOP₂PdS
Molecular Weight:909.115
Hs Code.:

trans-(PPh<sub>3</sub>)2Pd(C<sub>6</sub>H<sub>4</sub>-4-SC(O)Me)(I)

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Chemical Property of trans-(PPh₃)2Pd(C₆H₄-4-SC(O)Me)(I)

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Technology Process of trans-(PPh₃)2Pd(C₆H₄-4-SC(O)Me)(I)

There total 1 articles about trans-(PPh₃)2Pd(C₆H₄-4-SC(O)Me)(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 14221-01-3
tetrakis(triphenylphosphine) palladium⁽⁰⁾

: 69746-43-6
1-iodo-4-thioacetylbenzene

: 886970-58-7
trans-(PPh₃)2Pd(C₆H₄-4-SC(O)Me)(I)

Guidance literature:: In toluene; (under N2); ligand dissolved in toluene, Pd-complex added at 25°C, stirred for 24 h; volatiles removed in vac., dissolved in CH2Cl2, hexane added, decanted, washed with hexane; elem. anal.;
DOI:10.1016/j.ica.2005.08.033

Reference yield: 87.0%

: 886970-58-7
trans-(PPh₃)2Pd(C₆H₄-4-SC(O)Me)(I)

: 1591-30-6
(1,1'-biphenyl)-4,4'-dicarbonitrile

: 2923-28-6
silver trifluoromethanesulfonate

: [trans-(PPh₃)2Pd(C₆H₄-4-SC(O)Me)]2(4,4'-biphenyldicarbonitrile)(OTf)2

Guidance literature:: In dichloromethane; toluene; (under N2); AgCF3SO3 added to soln. of Pd-complex in toluene-CH2Cl2 at 25°C, stirred for 30 min, filtered, 4,4'-biphenyldicarbonitrile added, stirred for 30 min, hexane added; filtered, dried in vac.; elem. anal.;
DOI:10.1016/j.ica.2005.08.033

Reference yield: 86.0%

: 553-26-4
4,4'-bipyridine

: 886970-58-7
trans-(PPh₃)2Pd(C₆H₄-4-SC(O)Me)(I)

: 2923-28-6
silver trifluoromethanesulfonate

: [trans-(PPh₃)2Pd(C₆H₄-4-SC(O)Me)]2(4,4'-bipyridine)(OTf)2

Guidance literature:: In dichloromethane; toluene; (under N2); AgCF3SO3 added to soln. of Pd-complex in toluene-CH2Cl2 at 25°C, stirred for 30 min, filtered, 4,4'-bipyridine added, stirredfor 30 min, hexane added; filtered, dried in vac.; elem. anal.;
DOI:10.1016/j.ica.2005.08.033