phenylbis(3-thienyl)carbinol

Base Information

Chemical Name:phenylbis(3-thienyl)carbinol
CAS No.:133373-90-7
Molecular Formula:C₁₅H₁₂OS₂
Molecular Weight:272.392
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenylbis(3-thienyl)carbinol

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Technology Process of phenylbis(3-thienyl)carbinol

There total 1 articles about phenylbis(3-thienyl)carbinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

3-thienyl lithium: 1192-06-9
3-thienyl lithium

: 93-58-3,5705-52-2,80226-58-0
benzoic acid methyl ester

: 133373-90-7
phenylbis(3-thienyl)carbinol

Guidance literature:: In diethyl ether; 1) -70 deg C, 2 h, 2) rt, 50 h;
DOI:10.1021/jo00010a011

Reference yield: 70.0%

: 110-86-1
pyridine

: bis(trimethylsilyl)amide yttrium(III)

: 133373-90-7
phenylbis(3-thienyl)carbinol

: tris(phenylbis(3-thienyl)methanolate)bis(pyridine)yttrium(III)

Guidance literature:: In pyridine; toluene; (N2), 1 equiv. of Y complex in toluene and pyridine added to soln. of 3 equiv. of carbinol in toluene, stirred at room temp. for 2 d; crystd., filtered, elem. anal.;
DOI:10.1002/ejic.201101089