Toluene-4-sulfonic acid (R)-4-[(3R,5S,7R,8R,9S,10S,12S,13R,14S,17R)-10,13-dimethyl-3,7,12-tris-(tetrahydro-pyran-2-yloxy)-hexadecahydro-cyclopenta[a]phenanthren-17-yl]-pentyl ester

Base Information

Chemical Name:Toluene-4-sulfonic acid (R)-4-[(3R,5S,7R,8R,9S,10S,12S,13R,14S,17R)-10,13-dimethyl-3,7,12-tris-(tetrahydro-pyran-2-yloxy)-hexadecahydro-cyclopenta[a]phenanthren-17-yl]-pentyl ester
CAS No.:140681-11-4
Molecular Formula:C₄₆H₇₂O₉S
Molecular Weight:801.138
Hs Code.:

Toluene-4-sulfonic acid (R)-4-[(3R,5S,7R,8R,9S,10S,12S,13R,14S,17R)-10,13-dimethyl-3,7,12-tris-(tetrahydro-pyran-2-yloxy)-hexadecahydro-cyclopenta[a]phenanthren-17-yl]-pentyl ester

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Chemical Property of Toluene-4-sulfonic acid (R)-4-[(3R,5S,7R,8R,9S,10S,12S,13R,14S,17R)-10,13-dimethyl-3,7,12-tris-(tetrahydro-pyran-2-yloxy)-hexadecahydro-cyclopenta[a]phenanthren-17-yl]-pentyl ester

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Technology Process of Toluene-4-sulfonic acid (R)-4-[(3R,5S,7R,8R,9S,10S,12S,13R,14S,17R)-10,13-dimethyl-3,7,12-tris-(tetrahydro-pyran-2-yloxy)-hexadecahydro-cyclopenta[a]phenanthren-17-yl]-pentyl ester

There total 3 articles about Toluene-4-sulfonic acid (R)-4-[(3R,5S,7R,8R,9S,10S,12S,13R,14S,17R)-10,13-dimethyl-3,7,12-tris-(tetrahydro-pyran-2-yloxy)-hexadecahydro-cyclopenta[a]phenanthren-17-yl]-pentyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 81-25-4
cholic acid

: 140681-11-4
Toluene-4-sulfonic acid (R)-4-[(3R,5S,7R,8R,9S,10S,12S,13R,14S,17R)-10,13-dimethyl-3,7,12-tris-(tetrahydro-pyran-2-yloxy)-hexadecahydro-cyclopenta[a]phenanthren-17-yl]-pentyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: AcCl

2: p-TsOH / CH₂Cl₂

3: LiAlH₄ / tetrahydrofuran / Heating

4: 89 percent / pyridine

With pyridine; lithium aluminium tetrahydride; toluene-4-sulfonic acid; acetyl chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1248/cpb.46.12

Reference yield:

: 1448-36-8
methyl cholate

: 140681-11-4
Toluene-4-sulfonic acid (R)-4-[(3R,5S,7R,8R,9S,10S,12S,13R,14S,17R)-10,13-dimethyl-3,7,12-tris-(tetrahydro-pyran-2-yloxy)-hexadecahydro-cyclopenta[a]phenanthren-17-yl]-pentyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: p-TsOH / CH₂Cl₂

2: LiAlH₄ / tetrahydrofuran / Heating

3: 89 percent / pyridine

With pyridine; lithium aluminium tetrahydride; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1248/cpb.46.12

Reference yield:

: 140681-10-3
methyl 3α,7α,12α-tritetrahydropyran-2'-yloxy-5β-cholan-24-oate

: 140681-11-4
Toluene-4-sulfonic acid (R)-4-[(3R,5S,7R,8R,9S,10S,12S,13R,14S,17R)-10,13-dimethyl-3,7,12-tris-(tetrahydro-pyran-2-yloxy)-hexadecahydro-cyclopenta[a]phenanthren-17-yl]-pentyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / tetrahydrofuran / Heating

2: 89 percent / pyridine

With pyridine; lithium aluminium tetrahydride; In tetrahydrofuran;
DOI:10.1248/cpb.46.12