C₃₇H₄₀Cl₂N₆O

Base Information

Chemical Name:C₃₇H₄₀Cl₂N₆O
CAS No.:1049814-41-6
Molecular Formula:C₃₇H₄₀Cl₂N₆O
Molecular Weight:655.67
Hs Code.:

C<sub>37</sub>H<sub>40</sub>Cl<sub>2</sub>N<sub>6</sub>O

Synonyms:

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Chemical Property of C₃₇H₄₀Cl₂N₆O

Chemical Property:

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Technology Process of C₃₇H₄₀Cl₂N₆O

There total 11 articles about C₃₇H₄₀Cl₂N₆O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₂H₄₈Cl₂N₆O₃

: 1049814-41-6
C₃₇H₄₀Cl₂N₆O

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃;
DOI:10.1016/j.bmcl.2012.12.014

Reference yield:

: 1049809-51-9
3-(4-chloro-3-iodo-phenyl)-1,4,6,7-tetrahydro-pyrazolo[4,3-c]-pyridine-5-carboxylic acid tert-butyl ester

: 1049814-41-6
C₃₇H₄₀Cl₂N₆O

Guidance literature:: Multi-step reaction with 7 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 0 - 20 °C

2.1: trifluoroacetic acid / dichloromethane / 20 °C

3.1: N-ethyl-N,N-diisopropylamine; HATU; 1-hydroxy-7-aza-benzotriazole / N,N-dimethyl-formamide / 80 °C

4.1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 20 °C

5.1: Dess-Martin periodane / dichloromethane / 20 °C

6.1: acetic acid / dichloromethane

6.2: 0.5 h / 20 °C

7.1: trifluoroacetic acid / dichloromethane / 0 - 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 1-hydroxy-7-aza-benzotriazole; caesium carbonate; Dess-Martin periodane; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 4.1: |Sonogashira Cross-Coupling;
DOI:10.1016/j.bmcl.2012.12.014

Reference yield:

: 1049809-74-6
3-(4-Chloro-3-iodo-phenyl)-1-(3-hydroxy-propyl)-1,4,6,7-tetrahydro-pyrazolo[4,3-c]pyridine-5-carboxylic acid tert-butyl ester

: 1049814-41-6
C₃₇H₄₀Cl₂N₆O

Guidance literature:: Multi-step reaction with 6 steps

1.1: trifluoroacetic acid / dichloromethane / 20 °C

2.1: N-ethyl-N,N-diisopropylamine; HATU; 1-hydroxy-7-aza-benzotriazole / N,N-dimethyl-formamide / 80 °C

3.1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 20 °C

4.1: Dess-Martin periodane / dichloromethane / 20 °C

5.1: acetic acid / dichloromethane

5.2: 0.5 h / 20 °C

6.1: trifluoroacetic acid / dichloromethane / 0 - 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 1-hydroxy-7-aza-benzotriazole; Dess-Martin periodane; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 3.1: |Sonogashira Cross-Coupling;
DOI:10.1016/j.bmcl.2012.12.014