C₅₃H₇₂O₅S₂

Base Information

Chemical Name:C₅₃H₇₂O₅S₂
CAS No.:1370028-17-3
Molecular Formula:C₅₃H₇₂O₅S₂
Molecular Weight:853.284
Hs Code.:

C<sub>53</sub>H<sub>72</sub>O<sub>5</sub>S<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₃H₇₂O₅S₂

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of C₅₃H₇₂O₅S₂

There total 12 articles about C₅₃H₇₂O₅S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₃H₃₆O₃

: 1370028-17-3
C₅₃H₇₂O₅S₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / 0 °C / Inert atmosphere

1.2: 1 h / -78 °C / Inert atmosphere

2.1: toluene / 4.5 h / 120 °C / Inert atmosphere

3.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere

3.2: -78 °C / Inert atmosphere

4.1: Crabtree's catalyst; hydrogen / dichloromethane / 48 h / 20 °C / Inert atmosphere

5.1: trimethylaluminum / hexane; dichloromethane / 0.5 h / 0 °C / Inert atmosphere

5.2: 1 h / 0 °C / Inert atmosphere

6.1: tert.-butyl lithium / tetrahydrofuran; diethyl ether; pentane / 0.67 h / -78 °C / Inert atmosphere

6.2: 1.5 h / Inert atmosphere

7.1: zinc(II) chloride / dichloromethane / 0 - 20 °C / Inert atmosphere

8.1: lithium aluminium tetrahydride / diethyl ether / 0.25 h / 0 °C / Inert atmosphere

9.1: sodium hydride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

10.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 °C / Inert atmosphere

10.2: 0.08 h / 0 °C / Inert atmosphere

11.1: 0.5 h / 0 °C / Inert atmosphere

With lithium aluminium tetrahydride; n-butyllithium; Crabtree's catalyst; hydrogen; trimethylaluminum; tert.-butyl lithium; sodium hexamethyldisilazane; sodium hydride; N-ethyl-N,N-diisopropylamine; zinc(II) chloride; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; toluene; pentane; 7.1: Diels-Alder reaction;
DOI:10.1248/cpb.60.137

Reference yield:

: 1370028-21-9
C₄₁H₄₇NO₄S

: 1370028-17-3
C₅₃H₇₂O₅S₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: toluene / 7.5 h / 120 °C / Inert atmosphere

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere

2.2: -78 °C / Inert atmosphere

3.1: Crabtree's catalyst; hydrogen / dichloromethane / 48 h / 20 °C / Inert atmosphere

4.1: trimethylaluminum / hexane; dichloromethane / 0.5 h / 0 °C / Inert atmosphere

4.2: 1 h / 0 °C / Inert atmosphere

5.1: tert.-butyl lithium / tetrahydrofuran; diethyl ether; pentane / 0.67 h / -78 °C / Inert atmosphere

5.2: 1.5 h / Inert atmosphere

6.1: zinc(II) chloride / dichloromethane / 0 - 20 °C / Inert atmosphere

7.1: lithium aluminium tetrahydride / diethyl ether / 0.25 h / 0 °C / Inert atmosphere

8.1: sodium hydride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

9.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 °C / Inert atmosphere

9.2: 0.08 h / 0 °C / Inert atmosphere

10.1: 0.5 h / 0 °C / Inert atmosphere

With lithium aluminium tetrahydride; n-butyllithium; Crabtree's catalyst; hydrogen; trimethylaluminum; tert.-butyl lithium; sodium hexamethyldisilazane; sodium hydride; N-ethyl-N,N-diisopropylamine; zinc(II) chloride; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; toluene; pentane; 6.1: Diels-Alder reaction;
DOI:10.1248/cpb.60.137

Reference yield:

: 1370028-22-0
C₄₁H₄₇NO₄S

: 1370028-17-3
C₅₃H₇₂O₅S₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: toluene / 4.5 h / 120 °C / Inert atmosphere

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere

2.2: -78 °C / Inert atmosphere

3.1: Crabtree's catalyst; hydrogen / dichloromethane / 48 h / 20 °C / Inert atmosphere

4.1: trimethylaluminum / hexane; dichloromethane / 0.5 h / 0 °C / Inert atmosphere

4.2: 1 h / 0 °C / Inert atmosphere

5.1: tert.-butyl lithium / tetrahydrofuran; diethyl ether; pentane / 0.67 h / -78 °C / Inert atmosphere

5.2: 1.5 h / Inert atmosphere

6.1: zinc(II) chloride / dichloromethane / 0 - 20 °C / Inert atmosphere

7.1: lithium aluminium tetrahydride / diethyl ether / 0.25 h / 0 °C / Inert atmosphere

8.1: sodium hydride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

9.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 °C / Inert atmosphere

9.2: 0.08 h / 0 °C / Inert atmosphere

10.1: 0.5 h / 0 °C / Inert atmosphere

With lithium aluminium tetrahydride; n-butyllithium; Crabtree's catalyst; hydrogen; trimethylaluminum; tert.-butyl lithium; sodium hexamethyldisilazane; sodium hydride; N-ethyl-N,N-diisopropylamine; zinc(II) chloride; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; toluene; pentane; 6.1: Diels-Alder reaction;
DOI:10.1248/cpb.60.137