1,3-cyclooctadiene oxide

Base Information

• Chemical Name: 1,3-cyclooctadiene oxide
• CAS No.: 183904-03-2
• Molecular Formula: C₈H₁₂O
• Molecular Weight: 124.183
• Mol file: 183904-03-2.mol

Synonyms:

Chemical Property of 1,3-cyclooctadiene oxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3-cyclooctadiene oxide

There total 1 articles about 1,3-cyclooctadiene oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

1,3-cyclooctadiene (186983-16-4) → 1,3-cyclooctadiene oxide (6690-12-6,183904-03-2)

Guidance literature:

With peracetic acid; sodium carbonate; In dichloromethane; acetic acid; at 0 - 20 ℃; for 3h; Inert atmosphere;

DOI:10.1021/ol802104z

Reference yield:

1,3-cyclooctadiene oxide (6690-12-6,183904-03-2) → C15H17NO5

Guidance literature:

Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2: benzoic acid methyl ester / diethyl ether; cyclohexane / 10 h / 20 - 30 °C / UV-irradiation

3: pyridine / dichloromethane / 2 h / 20 °C / Inert atmosphere

With pyridine; benzoic acid methyl ester; lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; dichloromethane; cyclohexane;

upstream raw materials:

1,3-cyclooctadiene