(4-{[3-(9,10-Dioxo-9,10-dihydro-anthracen-2-yl)-2-(1H-indol-3-yl)-4-oxo-thiazolidin-5-ylmethyl]-amino}-phenyl)-acetic acid; hydrochloride

Base Information

Chemical Name:(4-{[3-(9,10-Dioxo-9,10-dihydro-anthracen-2-yl)-2-(1H-indol-3-yl)-4-oxo-thiazolidin-5-ylmethyl]-amino}-phenyl)-acetic acid; hydrochloride
CAS No.:108582-92-9
Molecular Formula:C₃₄H₂₅N₃O₅S*ClH
Molecular Weight:624.117
Hs Code.:

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Chemical Property of (4-{[3-(9,10-Dioxo-9,10-dihydro-anthracen-2-yl)-2-(1H-indol-3-yl)-4-oxo-thiazolidin-5-ylmethyl]-amino}-phenyl)-acetic acid; hydrochloride

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Technology Process of (4-{[3-(9,10-Dioxo-9,10-dihydro-anthracen-2-yl)-2-(1H-indol-3-yl)-4-oxo-thiazolidin-5-ylmethyl]-amino}-phenyl)-acetic acid; hydrochloride

There total 3 articles about (4-{[3-(9,10-Dioxo-9,10-dihydro-anthracen-2-yl)-2-(1H-indol-3-yl)-4-oxo-thiazolidin-5-ylmethyl]-amino}-phenyl)-acetic acid; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 5897-63-2
(4-amino-phenyl)-acetic acid ; hydrochloride

: 108582-84-9
2-<2-(1H-indol-3-yl)-4-oxo-3-thiazolidinyl>-9,10-anthracenedione

: 108582-92-9
(4-{[3-(9,10-Dioxo-9,10-dihydro-anthracen-2-yl)-2-(1H-indol-3-yl)-4-oxo-thiazolidin-5-ylmethyl]-amino}-phenyl)-acetic acid; hydrochloride

Guidance literature:: With hydrogenchloride; In methanol; for 3h; Heating;

Reference yield:

: 487-89-8,1228547-52-1
Indole-3-carboxaldehyde

: 108582-92-9
(4-{[3-(9,10-Dioxo-9,10-dihydro-anthracen-2-yl)-2-(1H-indol-3-yl)-4-oxo-thiazolidin-5-ylmethyl]-amino}-phenyl)-acetic acid; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) ZnCl₂ / 1.) DMF, 30 min, 2.) reflux, 7 h

2: 55 percent / conc. HCl / methanol / 3 h / Heating

With hydrogenchloride; zinc(II) chloride; In methanol;

Reference yield:

: 117-79-3
2-aminoanthraquinone

: 108582-92-9
(4-{[3-(9,10-Dioxo-9,10-dihydro-anthracen-2-yl)-2-(1H-indol-3-yl)-4-oxo-thiazolidin-5-ylmethyl]-amino}-phenyl)-acetic acid; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) ZnCl₂ / 1.) DMF, 30 min, 2.) reflux, 7 h

2: 55 percent / conc. HCl / methanol / 3 h / Heating

With hydrogenchloride; zinc(II) chloride; In methanol;