chloro[η5-(2-phenylthioethyl)cyclopentadienyl][η5-(2-phenylthioethyl)cyclopentadienyl-S]molybdenum hexafluorophosphate

Base Information

• Chemical Name: chloro[η5-(2-phenylthioethyl)cyclopentadienyl][η5-(2-phenylthioethyl)cyclopentadienyl-S]molybdenum hexafluorophosphate
• CAS No.: 86857-58-1
• Molecular Formula: C₂₆H₂₆ClMoS₂*F₆P
• Molecular Weight: 678.982
• Mol file: 86857-58-1.mol

Synonyms:

Chemical Property of chloro[η5-(2-phenylthioethyl)cyclopentadienyl][η5-(2-phenylthioethyl)cyclopentadienyl-S]molybdenum hexafluorophosphate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of chloro[η5-(2-phenylthioethyl)cyclopentadienyl][η5-(2-phenylthioethyl)cyclopentadienyl-S]molybdenum hexafluorophosphate

There total 1 articles about chloro[η5-(2-phenylthioethyl)cyclopentadienyl][η5-(2-phenylthioethyl)cyclopentadienyl-S]molybdenum hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

ammonium hexafluorophosphate + Mo(C5H4CH2CH2SC6H5)2Cl2 (86857-67-2) → chloro[η5-(2-phenylthioethyl)cyclopentadienyl][η5-(2-phenylthioethyl)cyclopentadienyl-S]molybdenum hexafluorophosphate (86857-58-1)

Guidance literature:

With FeCl₂*1.5THF; In tetrahydrofuran; water; FeCl2*1.5THF under inert gas added to Mo complex in THF, heated to 50°C for 1 h, evapd., extd. with H2O, filtered, excess aq. NH4PF6 added; washing with H2O, drying in vac., recrystn. (acetone-H2O); elem. anal.;

DOI:10.1039/DT9830000861

upstream raw materials:

Mo(C₅H₄CH₂CH₂SC₆H₅)2Cl₂