[Pr(5-nitroisophthalic acid(-2H))(1,10-phenanthroline)(N,N-dimethylformamide)(NO₃)](n)

Base Information

• Chemical Name: [Pr(5-nitroisophthalic acid(-2H))(1,10-phenanthroline)(N,N-dimethylformamide)(NO₃)](n)
• CAS No.: 922733-67-3
• Molecular Formula: C₃H₇NO*C₈H₃NO₆*C₁₂H₈N₂*NO₃*Pr
• Molecular Weight: 665.331
• Mol file: 922733-67-3.mol

Synonyms:

Chemical Property of [Pr(5-nitroisophthalic acid(-2H))(1,10-phenanthroline)(N,N-dimethylformamide)(NO₃)](n)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [Pr(5-nitroisophthalic acid(-2H))(1,10-phenanthroline)(N,N-dimethylformamide)(NO₃)](n)

There total 1 articles about [Pr(5-nitroisophthalic acid(-2H))(1,10-phenanthroline)(N,N-dimethylformamide)(NO₃)](n) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

1,10-Phenanthroline (66-71-7) + praseodymium(III) nitrate hexahydrate + 5-nitrobenzene-1,3-dicarboxylic acid (618-88-2) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → [Pr(5-nitroisophthalic acid(-2H))(1,10-phenanthroline)(N,N-dimethylformamide)(NO3)](n) (922733-67-3,943613-94-3)

Guidance literature:

In N,N-dimethyl-formamide; Pr salt dissolved in DMF; added dropwise to the mixt. of solns. of two ligands; placed in air for 6 mo; crystals were obtained; washed (anhyd. alc.); dried at room temp.; elem.anal.;

DOI:10.1007/s10973-005-7490-1

upstream raw materials:

1,10-Phenanthroline

5-nitrobenzene-1,3-dicarboxylic acid

N,N-dimethyl-formamide