C₂₄H₃₀N₄O₃S

Base Information

• Chemical Name: C₂₄H₃₀N₄O₃S
• CAS No.: 1374858-30-6
• Molecular Formula: C₂₄H₃₀N₄O₃S
• Molecular Weight: 454.593
• Mol file: 1374858-30-6.mol

Synonyms:

Chemical Property of C₂₄H₃₀N₄O₃S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₃₀N₄O₃S

There total 8 articles about C₂₄H₃₀N₄O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C14H19NO3 (1374859-11-6) + 5-amino-3-cyclohexyl-1,2-thiazole-4-carboxamide (1374858-21-5) → C24H30N4O3S (1374858-30-6)

Guidance literature:

With iodine; In N,N-dimethyl acetamide; at 130 ℃; for 1h;

DOI:10.1016/j.bmcl.2012.03.025

Reference yield:

[cyclohexyl(hydroxy)methylidene]propanedinitrile (553672-03-0) → C24H30N4O3S (1374858-30-6)

Guidance literature:

Multi-step reaction with 6 steps

1: trichlorophosphate / Reflux

2: ammonium hydroxide / 0.5 h / 20 °C

3: hydrogen sulfide; triethylamine / benzene

4: dihydrogen peroxide / methanol / 50 °C

5: sulfuric acid / 0.5 h / 80 °C

6: iodine / N,N-dimethyl acetamide / 1 h / 130 °C

With ammonium hydroxide; sulfuric acid; hydrogen sulfide; dihydrogen peroxide; iodine; triethylamine; trichlorophosphate; In methanol; N,N-dimethyl acetamide; benzene;

DOI:10.1016/j.bmcl.2012.03.025

Reference yield:

[chloro(cyclohexyl)methylidene]propanedinitrile → C24H30N4O3S (1374858-30-6)

Guidance literature:

Multi-step reaction with 5 steps

1: ammonium hydroxide / 0.5 h / 20 °C

2: hydrogen sulfide; triethylamine / benzene

3: dihydrogen peroxide / methanol / 50 °C

4: sulfuric acid / 0.5 h / 80 °C

5: iodine / N,N-dimethyl acetamide / 1 h / 130 °C

With ammonium hydroxide; sulfuric acid; hydrogen sulfide; dihydrogen peroxide; iodine; triethylamine; In methanol; N,N-dimethyl acetamide; benzene;

DOI:10.1016/j.bmcl.2012.03.025

upstream raw materials:

azepan-4-ol

4-fluoro-2-methoxybenzaldehyde

[cyclohexyl(hydroxy)methylidene]propanedinitrile

C₁₄H₁₉NO₃