cis-H{Ph₃Sn}Pt(PCy₃)2

Base Information

Chemical Name:cis-H{Ph₃Sn}Pt(PCy₃)2
CAS No.:118203-86-4
Molecular Formula:C₅₄H₈₂P₂PtSn
Molecular Weight:1106.98
Hs Code.:

cis-H{Ph<sub>3</sub>Sn}Pt(PCy<sub>3</sub>)2

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Chemical Property of cis-H{Ph₃Sn}Pt(PCy₃)2

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Technology Process of cis-H{Ph₃Sn}Pt(PCy₃)2

There total 4 articles about cis-H{Ph₃Sn}Pt(PCy₃)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.3%

: 55664-33-0
bis(tricyclohexylphosphine)platinum⁽⁰⁾

: 892-20-6
triphenylstannane

: 72742-25-7,118203-86-4
cis-H{Ph₃Sn}Pt(PCy₃)2

Guidance literature:: In hexane; under N2 atmosphere, in the dark, addn. of 1 equiv. of HSnPh3 to hexane soln. of Pt(PCy3)2, stirring for 3 h, pptn.; (1)H-NMR and (31)P-NMR spectroscopy, elem. anal.;

Reference yield: 84.4%

: (PCy₃)2PtO₂

: 892-20-6
triphenylstannane

: 118203-86-4,72742-25-7
trans-H(Ph₃Sn)Pt(PCy₃)2

Guidance literature:: In benzene; byproducts: oxygen; under N2 atmosphere, addn. of excess Ph3SnH to soln. of (PCy3)2PtO2 in dry benzene (evolution of O2), stirring for 1 h; removing of solvent, washing of residue with cold n-pentane, (31)P-NMR spectroscopy;

Reference yield:

: 55664-33-0
bis(tricyclohexylphosphine)platinum⁽⁰⁾

: 892-20-6
triphenylstannane

: 118203-86-4,72742-25-7
trans-H(Ph₃Sn)Pt(PCy₃)2

Guidance literature:: In hexane; under N2 atmosphere, dropwise addn. of HSnPh3 to hexane soln. of Pt(PCy3)2, stirring for 3 h, pptn., stirring for 12 h; filtration, (1)H- and (31)P-NMR spectroscopy, evapn. of solvent from supernatant, washing twice with cold n-pentane, pptn., elem. anal.;