2-(2-(((2S,6S,13S,E)-13-amino-2-(4-hydroxybenzyl)-4,14-dioxo-1,5-diazacyclotetradec-9-ene-6-carboxamido)methyl)phenyl)acetic acid trifluoroacetic acid salt

Base Information

Chemical Name:2-(2-(((2S,6S,13S,E)-13-amino-2-(4-hydroxybenzyl)-4,14-dioxo-1,5-diazacyclotetradec-9-ene-6-carboxamido)methyl)phenyl)acetic acid trifluoroacetic acid salt
CAS No.:1306746-16-6
Molecular Formula:C₂HF₃O₂*C₂₉H₃₆N₄O₆
Molecular Weight:650.652
Hs Code.:

2-(2-(((2S,6S,13S,E)-13-amino-2-(4-hydroxybenzyl)-4,14-dioxo-1,5-diazacyclotetradec-9-ene-6-carboxamido)methyl)phenyl)acetic acid trifluoroacetic acid salt

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Chemical Property of 2-(2-(((2S,6S,13S,E)-13-amino-2-(4-hydroxybenzyl)-4,14-dioxo-1,5-diazacyclotetradec-9-ene-6-carboxamido)methyl)phenyl)acetic acid trifluoroacetic acid salt

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Technology Process of 2-(2-(((2S,6S,13S,E)-13-amino-2-(4-hydroxybenzyl)-4,14-dioxo-1,5-diazacyclotetradec-9-ene-6-carboxamido)methyl)phenyl)acetic acid trifluoroacetic acid salt

There total 2 articles about 2-(2-(((2S,6S,13S,E)-13-amino-2-(4-hydroxybenzyl)-4,14-dioxo-1,5-diazacyclotetradec-9-ene-6-carboxamido)methyl)phenyl)acetic acid trifluoroacetic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1306746-03-1
2-(2-((5S,8S,12S)-5,12-di(but-3-en-1-yl)-1-(9H-fluoren-9-yl)-8-(4-hydroxybenzyl)-3,6,10,13-tetraoxo-2-oxa-4,7,11,14-tetraazapentadecan-15-yl)phenyl)acetic acid

: 1306746-16-6
2-(2-(((2S,6S,13S,E)-13-amino-2-(4-hydroxybenzyl)-4,14-dioxo-1,5-diazacyclotetradec-9-ene-6-carboxamido)methyl)phenyl)acetic acid trifluoroacetic acid salt

Guidance literature:: Multi-step reaction with 2 steps

1: Hoveyda-Grubbs catalyst second generation; p-benzoquinone / 1,2-dichloro-ethane / 0.08 h / 120 °C / Microwave irradiation

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile / 0.5 h

With Hoveyda-Grubbs catalyst second generation; 1,8-diazabicyclo[5.4.0]undec-7-ene; p-benzoquinone; In dimethyl sulfoxide; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm200036n

Reference yield:

: C₄₄H₄₆N₄O₈

: 76-05-1
trifluoroacetic acid

: 1306746-16-6
2-(2-(((2S,6S,13S,E)-13-amino-2-(4-hydroxybenzyl)-4,14-dioxo-1,5-diazacyclotetradec-9-ene-6-carboxamido)methyl)phenyl)acetic acid trifluoroacetic acid salt

Guidance literature:: C₄₄H₄₆N₄O₈; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile; for 0.5h;

trifluoroacetic acid; In water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm200036n