N-phenyl-8--2-oxo-8-azabicyclo<3.2.1>oct-3-ene-6,7-exo-dicarboximide

Base Information

• Chemical Name: N-phenyl-8--2-oxo-8-azabicyclo<3.2.1>oct-3-ene-6,7-exo-dicarboximide
• CAS No.: 74793-95-6
• Molecular Formula: C₂₄H₁₇ClN₂O₄
• Molecular Weight: 432.863

Synonyms:

Chemical Property of N-phenyl-8--2-oxo-8-azabicyclo<3.2.1>oct-3-ene-6,7-exo-dicarboximide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of N-phenyl-8--2-oxo-8-azabicyclo<3.2.1>oct-3-ene-6,7-exo-dicarboximide

There total 4 articles about N-phenyl-8--2-oxo-8-azabicyclo<3.2.1>oct-3-ene-6,7-exo-dicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.6%

N-phenyl-maleimide (941-69-5) + 1--3-oxidopyridinium (74780-48-6) → N-phenyl-8--2-oxo-8-azabicyclo<3.2.1>oct-3-ene-6,7-exo-dicarboximide (74793-95-6)

Guidance literature:

In acetonitrile; at 80 ℃; for 72h;

DOI:10.1039/P19800000362

Reference yield:

3-HYDROXYPYRIDINE (109-00-2) → N-phenyl-8--2-oxo-8-azabicyclo<3.2.1>oct-3-ene-6,7-exo-dicarboximide (74793-95-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 95.7 percent / tetrahydrofuran / 3 h / 20 °C

2: 94 percent / NEt₃ / acetonitrile

3: 11.6 percent / acetonitrile / 72 h / 80 °C

With triethylamine; In tetrahydrofuran; acetonitrile;

DOI:10.1039/P19800000362

Reference yield:

trans-1-(4-chlorophenyl)-3-chloroprop-2-en-1-one (15724-88-6) → N-phenyl-8--2-oxo-8-azabicyclo<3.2.1>oct-3-ene-6,7-exo-dicarboximide (74793-95-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 95.7 percent / tetrahydrofuran / 3 h / 20 °C

2: 94 percent / NEt₃ / acetonitrile

3: 11.6 percent / acetonitrile / 72 h / 80 °C

With triethylamine; In tetrahydrofuran; acetonitrile;

DOI:10.1039/P19800000362

upstream raw materials:

N-phenyl-maleimide

1--3-oxidopyridinium

3-HYDROXYPYRIDINE

trans-1-(4-chlorophenyl)-3-chloroprop-2-en-1-one

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