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VOCl2(OC6H4C(C6H5)NOH)

Base Information
  • Chemical Name:VOCl2(OC6H4C(C6H5)NOH)
  • CAS No.:152952-31-3
  • Molecular Formula:C13H10Cl2NO3V
  • Molecular Weight:350.075
  • Hs Code.:
VOCl<sub>2</sub>(OC<sub>6</sub>H<sub>4</sub>C(C<sub>6</sub>H<sub>5</sub>)NOH)

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Chemical Property of VOCl2(OC6H4C(C6H5)NOH)
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Technology Process of VOCl2(OC6H4C(C6H5)NOH)

There total 1 articles about VOCl2(OC6H4C(C6H5)NOH) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In dichloromethane; treating a soln. of ligand in CH2Cl2 with VOCl3; keeping at 0°C for 72 h, pptn., washing repeatedly with cold EtOH/dioxane, drying under N2 over P4O10, elem. anal.;
Guidance literature:
With pyridine; In pyridine; treating a soln. of ligand with pyridine, keeping at 70°C for 15 min; evapn. of solvent, washing repeatedly with cold EtOH, drying under N2 over P4O10, elem. anal.;
Guidance literature:
With methanol; In methanol; heating a soln. of V-complex in MeOH and triethyl orthoformate on a stem bath under an air condenser, rotating for 30 min; evapn. of solvent, washing repeatedly with cold MeOH, drying under N2 over P4O10, elem. anal.;
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