(Rh(C₈H₁₂)(C(P(C₆H₅)2)(P(S)(C₆H₅)2)2))*CH₂Cl₂

Base Information

Chemical Name:(Rh(C₈H₁₂)(C(P(C₆H₅)2)(P(S)(C₆H₅)2)2))*CH₂Cl₂
CAS No.:153218-58-7
Molecular Formula:CH₂Cl₂*C₄₅H₄₂P₃RhS₂
Molecular Weight:927.72
Hs Code.:

(Rh(C<sub>8</sub>H<sub>12</sub>)(C(P(C<sub>6</sub>H<sub>5</sub>)2)(P(S)(C<sub>6</sub>H<sub>5</sub>)2)2))*CH<sub>2</sub>Cl<sub>2</sub>

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Chemical Property of (Rh(C₈H₁₂)(C(P(C₆H₅)2)(P(S)(C₆H₅)2)2))*CH₂Cl₂

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Technology Process of (Rh(C₈H₁₂)(C(P(C₆H₅)2)(P(S)(C₆H₅)2)2))*CH₂Cl₂

There total 1 articles about (Rh(C₈H₁₂)(C(P(C₆H₅)2)(P(S)(C₆H₅)2)2))*CH₂Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 12092-47-6
di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium

: 75425-87-5
bis(diphenylthiophosphoryl)diphenylphosphinomethane

: 153218-58-7
(Rh(C₈H₁₂)(C(P(C₆H₅)2)(P(S)(C₆H₅)2)2))*CH₂Cl₂

Guidance literature:: With HNEt₂; In dichloromethane; addn. of ligand to a stirred soln. of Rh-complex in CH2Cl2 at room temp. under dry N2, addn. of HNEt2, reacting for 10 min; removal of solvent in vacuo, extn. with toluene, removal of solvent from the extract in vacuo, recrystn. from CH2Cl2/hexane, elem. anal.;
DOI:10.1016/0022-328X(93)80367-K

Reference yield: 80.0%

: 153218-58-7
(Rh(C₈H₁₂)(C(P(C₆H₅)2)(P(S)(C₆H₅)2)2))*CH₂Cl₂

: 119072-55-8,7188-38-7
tert-butylisonitrile

: (Rh((CH₃)3CNC)2(C(P(C₆H₅)2)(P(S)(C₆H₅)2)2))*CH₂Cl₂

Guidance literature:: With HNEt₂; In dichloromethane; dropwise addn. of a soln. of ligand in CH2Cl2 to a stirred soln. of Rh-complex in CH2Cl2 at room temp. under dry N2, reacting for 5 min; removal of solvent in vacuo, crystn. from CH2Cl2-soln. of residue by layering with hexane, elem. anal.;
DOI:10.1016/0022-328X(93)80367-K