Diisopropyl-phosphoramidous acid 2-cyano-ethyl ester (2R,3S,5R)-5-formylamino-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-3-yl ester

Base Information

• Chemical Name: Diisopropyl-phosphoramidous acid 2-cyano-ethyl ester (2R,3S,5R)-5-formylamino-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-3-yl ester
• CAS No.: 135878-60-3
• Molecular Formula: C₃₅H₄₄N₃O₆P
• Molecular Weight: 633.725

Synonyms:

Chemical Property of Diisopropyl-phosphoramidous acid 2-cyano-ethyl ester (2R,3S,5R)-5-formylamino-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-3-yl ester

Chemical Property:

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Technology Process of Diisopropyl-phosphoramidous acid 2-cyano-ethyl ester (2R,3S,5R)-5-formylamino-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-3-yl ester

There total 1 articles about Diisopropyl-phosphoramidous acid 2-cyano-ethyl ester (2R,3S,5R)-5-formylamino-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

N,N,N',N'-tetraisopropyl 2-cyanoethylphosphorodiamidite (102691-36-1) + N-{(2R,4S,5R)-4-Hydroxy-5-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-2-yl}-formamide → Diisopropyl-phosphoramidous acid 2-cyano-ethyl ester (2R,3S,5R)-5-formylamino-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-3-yl ester (135878-60-3)

Guidance literature:

With 1H-tetrazole; In dichloromethane;

DOI:10.1016/0040-4039(95)01950-M

Reference yield:

Diisopropyl-phosphoramidous acid 2-cyano-ethyl ester (2R,3S,5R)-5-formylamino-2-hydroxymethyl-tetrahydro-furan-3-yl ester + Diisopropyl-phosphoramidous acid 2-cyano-ethyl ester (2R,3S,5R)-5-formylamino-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-3-yl ester (135878-60-3) → C88H123N12O61P9

Guidance literature:

Yield given. Multistep reaction;

DOI:10.1016/0040-4039(95)01950-M

upstream raw materials:

N,N,N',N'-tetraisopropyl 2-cyanoethylphosphorodiamidite

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