N-benzyl,N-(5,5-dimethyl-3-oxo-cyclohex-1-enyl)-2-aminoacetamide

Base Information

Chemical Name:N-benzyl,N-(5,5-dimethyl-3-oxo-cyclohex-1-enyl)-2-aminoacetamide
CAS No.:175469-08-6
Molecular Formula:C₂₈H₃₄N₂O₂
Molecular Weight:430.59
Hs Code.:

N-benzyl,N-(5,5-dimethyl-3-oxo-cyclohex-1-enyl)-2-<allyl,1-(phenyl)ethyl>aminoacetamide

Synonyms:

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Chemical Property of N-benzyl,N-(5,5-dimethyl-3-oxo-cyclohex-1-enyl)-2-aminoacetamide

Chemical Property:

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Technology Process of N-benzyl,N-(5,5-dimethyl-3-oxo-cyclohex-1-enyl)-2-aminoacetamide

There total 4 articles about N-benzyl,N-(5,5-dimethyl-3-oxo-cyclohex-1-enyl)-2-aminoacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3471-13-4
dimedone

: 175469-08-6
N-benzyl,N-(5,5-dimethyl-3-oxo-cyclohex-1-enyl)-2-aminoacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / p-toluenesulfonic acid / toluene / 10 h / Heating

2: 1.) NaHMDS / 1.) THF, -78 deg C, 5 h, 2.) THF, RT, overnight

3: K₂CO₃ / acetonitrile / Heating

With sodium hexamethyldisilazane; potassium carbonate; toluene-4-sulfonic acid; In toluene; acetonitrile;
DOI:10.1016/0040-4020(95)01090-4

Reference yield:

: 889-31-6
5,5-dimethyl-3-benzylamino-2-cyclohexen-1-one

: 175469-08-6
N-benzyl,N-(5,5-dimethyl-3-oxo-cyclohex-1-enyl)-2-aminoacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaHMDS / 1.) THF, -78 deg C, 5 h, 2.) THF, RT, overnight

2: K₂CO₃ / acetonitrile / Heating

With sodium hexamethyldisilazane; potassium carbonate; In acetonitrile;
DOI:10.1016/0040-4020(95)01090-4

Reference yield:

: 100-46-9
benzylamine

: 175469-08-6
N-benzyl,N-(5,5-dimethyl-3-oxo-cyclohex-1-enyl)-2-aminoacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / p-toluenesulfonic acid / toluene / 10 h / Heating

2: 1.) NaHMDS / 1.) THF, -78 deg C, 5 h, 2.) THF, RT, overnight

3: K₂CO₃ / acetonitrile / Heating

With sodium hexamethyldisilazane; potassium carbonate; toluene-4-sulfonic acid; In toluene; acetonitrile;
DOI:10.1016/0040-4020(95)01090-4