2,2'-Dicyano-3,3'-bis

Base Information

• Chemical Name: 2,2'-Dicyano-3,3'-bis
• CAS No.: 51796-62-4
• Molecular Formula: C₁₈H₁₀N₄
• Molecular Weight: 282.304

Synonyms:

Chemical Property of 2,2'-Dicyano-3,3'-bis

Chemical Property:

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Technology Process of 2,2'-Dicyano-3,3'-bis

There total 2 articles about 2,2'-Dicyano-3,3'-bis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

2-Azidoquinoline 1-oxide (51796-60-2) → 2-Amino-chinolin-1-oxid (30958-68-0) + 2-Cyanoisatogen (51796-61-3) + 2,2'-Dicyano-3,3'-bis (51796-62-4)

Guidance literature:

In methanol; at 85 ℃; for 3h; Product distribution; toluene, 100 deg C, 15 min;

DOI:10.1021/jo01314a020

Reference yield: 22.0%

1H-indole-2-carbonitrile (36193-65-4) → 3-iodo-1H-indole-2-carbonitrile (51796-65-7) + 2,2'-Dicyano-3,3'-bis (51796-62-4)

Guidance literature:

With iodine; In xylene; 1.) 140 deg C, 6 h, 2.) cooling, 10 h;

DOI:10.1021/jo01314a020

upstream raw materials:

1H-indole-2-carbonitrile

2-Azidoquinoline 1-oxide

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