Technology Process of trans-4-[6-(tetrahydropyran-2-yloxy)hexyloxy]cyclohexanecarbonyl methanesulfonate
There total 7 articles about trans-4-[6-(tetrahydropyran-2-yloxy)hexyloxy]cyclohexanecarbonyl methanesulfonate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridinium 4-toluenesulfonate / CH2Cl2 / 24 h / Ambient temperature
2: 30 g / potassium hydroxide / H2O / 3 h / Heating
3: triethylamine / CH2Cl2 / 3 h
With
potassium hydroxide; pyridinium p-toluenesulfonate; triethylamine;
In
dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 75 percent / sodium methoxide, sodium iodide / ethanol / 16 h / Heating
2: 60 percent / sodium hydroxide, potassium hydroxide / ethanol; H2O / 1 h / 200 °C
3: pyridinium 4-toluenesulfonate / CH2Cl2 / 24 h / Ambient temperature
4: 30 g / potassium hydroxide / H2O / 3 h / Heating
5: triethylamine / CH2Cl2 / 3 h
With
potassium hydroxide; sodium hydroxide; sodium methylate; pyridinium p-toluenesulfonate; triethylamine; sodium iodide;
In
ethanol; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 75 percent / sodium methoxide, sodium iodide / ethanol / 16 h / Heating
2: 60 percent / sodium hydroxide, potassium hydroxide / ethanol; H2O / 1 h / 200 °C
3: pyridinium 4-toluenesulfonate / CH2Cl2 / 24 h / Ambient temperature
4: 30 g / potassium hydroxide / H2O / 3 h / Heating
5: triethylamine / CH2Cl2 / 3 h
With
potassium hydroxide; sodium hydroxide; sodium methylate; pyridinium p-toluenesulfonate; triethylamine; sodium iodide;
In
ethanol; dichloromethane; water;
