1-[6-Hydroxy-2-(4-methoxybenzoyl)-3-methyl-1-benzofuran-5-yl]ethan-1-one

Base Information

Chemical Name:1-[6-Hydroxy-2-(4-methoxybenzoyl)-3-methyl-1-benzofuran-5-yl]ethan-1-one
CAS No.:106206-63-7
Molecular Formula:C19H16O5
Molecular Weight:324.333
Hs Code.:
DSSTox Substance ID:DTXSID10544708
Wikidata:Q82421935

Synonyms:106206-63-7;1-(6-Hydroxy-2-(4-methoxybenzoyl)-3-methylbenzofuran-5-yl)ethanone;DTXSID10544708;1-[6-Hydroxy-2-(4-methoxybenzoyl)-3-methyl-1-benzofuran-5-yl]ethan-1-one

Suppliers and Price of 1-[6-Hydroxy-2-(4-methoxybenzoyl)-3-methyl-1-benzofuran-5-yl]ethan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1-[6-Hydroxy-2-(4-methoxybenzoyl)-3-methyl-1-benzofuran-5-yl]ethan-1-one

Chemical Property:

XLogP3:4.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:324.09977361
Heavy Atom Count:24
Complexity:482

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(OC2=CC(=C(C=C12)C(=O)C)O)C(=O)C3=CC=C(C=C3)OC

Technology Process of 1-[6-Hydroxy-2-(4-methoxybenzoyl)-3-methyl-1-benzofuran-5-yl]ethan-1-one

There total 1 articles about 1-[6-Hydroxy-2-(4-methoxybenzoyl)-3-methyl-1-benzofuran-5-yl]ethan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 2161-85-5
1-(5-acetyl-2,4-dihydroxyphenyl)-1-ethanone

: 2632-13-5
2-Bromo-4'-methoxyacetophenone

: 106206-63-7
2-(p-methoxybenzoyl)-3-methyl-5-acetyl-6-hydroxybenzofuran

Guidance literature:: With potassium carbonate; In acetone; for 6h; Heating;

Reference yield: 70.0%

: 114-70-5
sodium phenylacetate

: 106206-63-7
2-(p-methoxybenzoyl)-3-methyl-5-acetyl-6-hydroxybenzofuran

: 106536-43-0
2-(p-methoxybenzoyl)-3,5-dimethyl-6-phenyl-7H-furo<3,2-g><1>benzopyran-7-one

Guidance literature:: With acetic anhydride; for 24h; Heating;
DOI:10.1246/bcsj.59.1299

Reference yield:

: 106206-63-7
2-(p-methoxybenzoyl)-3-methyl-5-acetyl-6-hydroxybenzofuran

: 2-[4-(2-Dimethylamino-ethoxy)-benzoyl]-3,5-dimethyl-6-phenyl-furo[3,2-g]chromen-7-one

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / Ac₂O / 24 h / Heating

2: 90 percent / pyridine hydrochloride / 0.5 h / Heating

3: K₂CO₃ / acetone / 20 h / Heating

With pyridine hydrochloride; acetic anhydride; potassium carbonate; In acetone;
DOI:10.1246/bcsj.59.1299