C₁₆H₁₈F₃NO₅S₂

Base Information

Chemical Name:C₁₆H₁₈F₃NO₅S₂
CAS No.:1374550-62-5
Molecular Formula:C₁₆H₁₈F₃NO₅S₂
Molecular Weight:425.45
Hs Code.:

C<sub>16</sub>H<sub>18</sub>F<sub>3</sub>NO<sub>5</sub>S<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₁₈F₃NO₅S₂

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of C₁₆H₁₈F₃NO₅S₂

There total 8 articles about C₁₆H₁₈F₃NO₅S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 37595-74-7
N,N-phenylbistrifluoromethane-sulfonimide

: 1374550-81-8
C₁₅H₁₉NO₃S

: 1374550-62-5
C₁₆H₁₈F₃NO₅S₂

Guidance literature:: C₁₅H₁₉NO₃S; With lithium hexamethyldisilazane; In tetrahydrofuran; ethylbenzene; at -78 ℃; for 0.583333h; Inert atmosphere;

N,N-phenylbistrifluoromethane-sulfonimide; In tetrahydrofuran; ethylbenzene; at -78 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/asia.201101029

Reference yield:

: 1374550-49-8
N-(4-(1-hydroxycyclobutyl)but-3-yn-1-yl)-4-methylbenzenesulfonamide

: 1374550-62-5
C₁₆H₁₈F₃NO₅S₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: trifluoromethanesulfonyloxy(triphenylphosphine)gold(I); toluene-4-sulfonic acid / dichloromethane / 4 h / 25 °C / Molecular sieve; Darkness

2.1: lithium hexamethyldisilazane / tetrahydrofuran; ethylbenzene / 0.58 h / -78 °C / Inert atmosphere

2.2: 2 h / -78 - 20 °C / Inert atmosphere

With trifluoromethanesulfonyloxy(triphenylphosphine)gold(I); toluene-4-sulfonic acid; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; ethylbenzene;
DOI:10.1002/asia.201101029

Reference yield:

: 1374550-54-5
1-(4-hydroxybut-1-yn-1-yl)cyclobutan-1-ol

: 1374550-62-5
C₁₆H₁₈F₃NO₅S₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

2.1: hydrazine hydrate / ethanol / 3 h / Reflux

3.1: triethylamine / dichloromethane / 0.67 h / 0 °C / Inert atmosphere

4.1: trifluoromethanesulfonyloxy(triphenylphosphine)gold(I); toluene-4-sulfonic acid / dichloromethane / 4 h / 25 °C / Molecular sieve; Darkness

5.1: lithium hexamethyldisilazane / tetrahydrofuran; ethylbenzene / 0.58 h / -78 °C / Inert atmosphere

5.2: 2 h / -78 - 20 °C / Inert atmosphere

With trifluoromethanesulfonyloxy(triphenylphosphine)gold(I); di-isopropyl azodicarboxylate; toluene-4-sulfonic acid; hydrazine hydrate; triethylamine; triphenylphosphine; lithium hexamethyldisilazane; In tetrahydrofuran; ethanol; dichloromethane; ethylbenzene; 1.1: Mitsunobu reaction;
DOI:10.1002/asia.201101029