Dihydrochloride Sal t of N-(4-(4?'-guanidinophenyl)phenylethylene)-4-aminooctanamidee

Base Information

• Chemical Name: Dihydrochloride Sal t of N-(4-(4?'-guanidinophenyl)phenylethylene)-4-aminooctanamidee
• CAS No.: 5715-27-5
• Molecular Formula: C₈H₁₂
• Molecular Weight: 108.183
• Mol file: 5715-27-5.mol

Synonyms:

Chemical Property of Dihydrochloride Sal t of N-(4-(4?'-guanidinophenyl)phenylethylene)-4-aminooctanamidee

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Dihydrochloride Sal t of N-(4-(4?'-guanidinophenyl)phenylethylene)-4-aminooctanamidee

There total 5 articles about Dihydrochloride Sal t of N-(4-(4?'-guanidinophenyl)phenylethylene)-4-aminooctanamidee which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

buta-1,3-diene (106-99-0,130983-70-9,29406-96-0,9003-17-2) → Dihydrochloride Sal t of N-(4-(4?'-guanidinophenyl)phenylethylene)-4-aminooctanamidee (5715-27-5)

Guidance literature:

With Fuller's Earth; at 300 - 400 ℃;

Reference yield:

3-methyl-4-formylcyclohexene (17775-58-5) → Dihydrochloride Sal t of N-(4-(4?'-guanidinophenyl)phenylethylene)-4-aminooctanamidee (5715-27-5)

Guidance literature:

Multi-step reaction with 3 steps

1: (i) N₂H₄, diethylene glycol, (ii) KOH

2: NBS / CCl₄

3: (i) EtMgBr, Et₂O, (ii) Na

With N-Bromosuccinimide; In tetrachloromethane;

DOI:10.1007/BF00850331

Reference yield:

2,3-Dimethyl-cyclohexen (2808-72-2) → Dihydrochloride Sal t of N-(4-(4?'-guanidinophenyl)phenylethylene)-4-aminooctanamidee (5715-27-5)

Guidance literature:

Multi-step reaction with 2 steps

1: NBS / CCl₄

2: (i) EtMgBr, Et₂O, (ii) Na

With N-Bromosuccinimide; In tetrachloromethane;

DOI:10.1007/BF00850331

upstream raw materials:

buta-1,3-diene

6-Brom-3,4-dimethyl-cyclohexen

3-methyl-4-formylcyclohexene

2,3-Dimethyl-cyclohexen