[1-¹⁴C]-o-chlorobenzylidenemalononitrile

Base Information

Chemical Name:[1-¹⁴C]-o-chlorobenzylidenemalononitrile
CAS No.:67297-65-8
Molecular Formula:C₁₀H₅ClN₂
Molecular Weight:190.605
Hs Code.:

[1-<sup>14</sup>C]-o-chlorobenzylidenemalononitrile

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [1-¹⁴C]-o-chlorobenzylidenemalononitrile

Chemical Property:

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Technology Process of [1-¹⁴C]-o-chlorobenzylidenemalononitrile

There total 5 articles about [1-¹⁴C]-o-chlorobenzylidenemalononitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 62-53-3
aniline

: 67297-65-8
[1-¹⁴C]-o-chlorobenzylidenemalononitrile

Guidance literature:: Multi-step reaction with 5 steps

1: potassium iodide / water

2: magnesium / diethyl ether

3: lithium aluminium tetrahydride / diethyl ether / 1 h / 20 °C

4: dinitrogen tetraoxide / 18 h / 20 °C

5: methanol / 3 h

With lithium aluminium tetrahydride; dinitrogen tetraoxide; magnesium; potassium iodide; In methanol; diethyl ether; water; 4: |Pfitzner-Moffatt Oxidation;
DOI:10.1002/jlcr.2580140118

Reference yield:

: 615-41-8
2-iodochlorobenzene

: 67297-65-8
[1-¹⁴C]-o-chlorobenzylidenemalononitrile

Guidance literature:: Multi-step reaction with 4 steps

1: magnesium / diethyl ether

2: lithium aluminium tetrahydride / diethyl ether / 1 h / 20 °C

3: dinitrogen tetraoxide / 18 h / 20 °C

4: methanol / 3 h

With lithium aluminium tetrahydride; dinitrogen tetraoxide; magnesium; In methanol; diethyl ether; 3: |Pfitzner-Moffatt Oxidation;
DOI:10.1002/jlcr.2580140118

Reference yield:

: 40681-65-0
o-chlorobenzoic [¹⁴C]acid

: 67297-65-8
[1-¹⁴C]-o-chlorobenzylidenemalononitrile

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / diethyl ether / 1 h / 20 °C

2: dinitrogen tetraoxide / 18 h / 20 °C

3: methanol / 3 h

With lithium aluminium tetrahydride; dinitrogen tetraoxide; In methanol; diethyl ether; 2: |Pfitzner-Moffatt Oxidation;
DOI:10.1002/jlcr.2580140118