C₅₅H₇₂N₂O₁₁SSi

Base Information

Chemical Name:C₅₅H₇₂N₂O₁₁SSi
CAS No.:217175-27-4
Molecular Formula:C₅₅H₇₂N₂O₁₁SSi
Molecular Weight:997.335
Hs Code.:

C<sub>55</sub>H<sub>72</sub>N<sub>2</sub>O<sub>11</sub>SSi

Synonyms:

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Chemical Property of C₅₅H₇₂N₂O₁₁SSi

Chemical Property:

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Technology Process of C₅₅H₇₂N₂O₁₁SSi

There total 16 articles about C₅₅H₇₂N₂O₁₁SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18303-04-3
N-[(tert-butoxy)carbonyl]-4-methylbenzenesulfonamide

: 217175-27-4
C₅₅H₇₂N₂O₁₁SSi

Guidance literature:: Multi-step reaction with 11 steps

1.1: Ph₃P; DEAD / tetrahydrofuran

2.1: n-BuLi / diethyl ether

3.1: H₂ / Pd/CaCO₃/Pb / toluene

4.1: lithium hexamethyldisilazane / tetrahydrofuran; 1,2-dimethoxy-ethane / -78 °C

4.2: 71 percent / tetrahydrofuran; 1,2-dimethoxy-ethane / -78 °C

5.1: 69 percent / dimethylsulfoxide / 180 °C

6.1: 91 percent / Me₃Al / toluene

7.1: LHMDS / tetrahydrofuran / -78 °C

7.2: 79 percent / N,N-dimethylpropylene urea / tetrahydrofuran / -78 °C

8.1: 75 percent / aq. HCl / tetrahydrofuran

9.1: 98 percent / DMAP / acetonitrile

10.1: DIBALH / CH₂Cl₂ / -78 °C

11.1: NaCNBH₃ / acetic acid

With hydrogenchloride; dmap; n-butyllithium; hydrogen; trimethylaluminum; diisobutylaluminium hydride; sodium cyanoborohydride; triphenylphosphine; lithium hexamethyldisilazane; diethylazodicarboxylate; Lindlar's catalyst; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; dichloromethane; acetic acid; dimethyl sulfoxide; toluene; acetonitrile; 1.1: Alkylation / 2.1: Acylation / 3.1: Catalytic hydrogenation / 4.1: Metallation / 4.2: Michael addition / 5.1: Elimination / 6.1: Cyclization / 7.1: Metallation / 7.2: Alkylation / 8.1: Hydrolysis / 9.1: Acylation / 10.1: Reduction / 11.1: Reduction;
DOI:10.1021/jo9817117

Reference yield:

: 101924-53-2
diethyl (2S,3R)-2-azido-3-hydroxysuccinate

: 217175-27-4
C₅₅H₇₂N₂O₁₁SSi

Guidance literature:: Multi-step reaction with 12 steps

1.1: 54 percent / BH₃*Me₂S; NaBH₄ / tetrahydrofuran

2.1: 82 percent / imidazole / tetrahydrofuran

3.1: H₂ / Pd/C / ethyl acetate

4.1: CH₂Cl₂

5.1: lithium hexamethyldisilazane / tetrahydrofuran; 1,2-dimethoxy-ethane / -78 °C

5.2: 71 percent / tetrahydrofuran; 1,2-dimethoxy-ethane / -78 °C

6.1: 69 percent / dimethylsulfoxide / 180 °C

7.1: 91 percent / Me₃Al / toluene

8.1: LHMDS / tetrahydrofuran / -78 °C

8.2: 79 percent / N,N-dimethylpropylene urea / tetrahydrofuran / -78 °C

9.1: 75 percent / aq. HCl / tetrahydrofuran

10.1: 98 percent / DMAP / acetonitrile

11.1: DIBALH / CH₂Cl₂ / -78 °C

12.1: NaCNBH₃ / acetic acid

With 1H-imidazole; hydrogenchloride; dmap; sodium tetrahydroborate; dimethylsulfide borane complex; hydrogen; trimethylaluminum; diisobutylaluminium hydride; sodium cyanoborohydride; lithium hexamethyldisilazane; palladium on activated charcoal; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; acetic acid; dimethyl sulfoxide; ethyl acetate; toluene; acetonitrile; 1.1: Reduction / 2.1: silylation / 3.1: Catalytic hydrogenation / 4.1: Cyclization / 5.1: Metallation / 5.2: Michael addition / 6.1: Elimination / 7.1: Cyclization / 8.1: Metallation / 8.2: Alkylation / 9.1: Hydrolysis / 10.1: Acylation / 11.1: Reduction / 12.1: Reduction;
DOI:10.1021/jo9817117

Reference yield:

: 101924-56-5
(2S,3R)-ethyl 2-azido-3,4-dihydroxybutanoate

: 217175-27-4
C₅₅H₇₂N₂O₁₁SSi

Guidance literature:: Multi-step reaction with 11 steps

1.1: 82 percent / imidazole / tetrahydrofuran

2.1: H₂ / Pd/C / ethyl acetate

3.1: CH₂Cl₂

4.1: lithium hexamethyldisilazane / tetrahydrofuran; 1,2-dimethoxy-ethane / -78 °C

4.2: 71 percent / tetrahydrofuran; 1,2-dimethoxy-ethane / -78 °C

5.1: 69 percent / dimethylsulfoxide / 180 °C

6.1: 91 percent / Me₃Al / toluene

7.1: LHMDS / tetrahydrofuran / -78 °C

7.2: 79 percent / N,N-dimethylpropylene urea / tetrahydrofuran / -78 °C

8.1: 75 percent / aq. HCl / tetrahydrofuran

9.1: 98 percent / DMAP / acetonitrile

10.1: DIBALH / CH₂Cl₂ / -78 °C

11.1: NaCNBH₃ / acetic acid

With 1H-imidazole; hydrogenchloride; dmap; hydrogen; trimethylaluminum; diisobutylaluminium hydride; sodium cyanoborohydride; lithium hexamethyldisilazane; palladium on activated charcoal; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; acetic acid; dimethyl sulfoxide; ethyl acetate; toluene; acetonitrile; 1.1: silylation / 2.1: Catalytic hydrogenation / 3.1: Cyclization / 4.1: Metallation / 4.2: Michael addition / 5.1: Elimination / 6.1: Cyclization / 7.1: Metallation / 7.2: Alkylation / 8.1: Hydrolysis / 9.1: Acylation / 10.1: Reduction / 11.1: Reduction;
DOI:10.1021/jo9817117