[(tBuC(NDipp-κ1N)(η3-NDipp))ZnMe]

Base Information

Chemical Name:[(tBuC(NDipp-κ1N)(η3-NDipp))ZnMe]
CAS No.:1256380-63-8
Molecular Formula:C₃₀H₄₆N₂Zn
Molecular Weight:500.099
Hs Code.:

Synonyms:

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Chemical Property of [(tBuC(NDipp-κ1N)(η3-NDipp))ZnMe]

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Technology Process of [(tBuC(NDipp-κ1N)(η3-NDipp))ZnMe]

There total 1 articles about [(tBuC(NDipp-κ1N)(η3-NDipp))ZnMe] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 544-97-8
dimethyl zinc(II)

: 630111-11-4,865200-87-9,1256380-68-3
N,N'-bis(2,6-diisopropylphenyl)(tert-butyl)amidine

: 1256380-63-8
[(tBuC(NDipp-κ1N)(η3-NDipp))ZnMe]

Guidance literature:: In toluene; byproducts: CH4; (inert atm.); addn. of toluene soln. of dimethylzinc to toluene soln. ofamidine deriv. at room temp., stirring for 2 h; concg., keeping at -30°C for 24 h, isolation of crystals, elem. anal.;
DOI:10.1021/om1008549

Reference yield: 90.0%

: 3978-81-2
4-tert-butylpyridine

: 1256380-63-8
[(tBuC(NDipp-κ1N)(η3-NDipp))ZnMe]

: 1256380-66-1
[(tBuC(NDipp)2-N,N')ZnMe(4-tert-butylpyridine)]

Guidance literature:: In toluene; (inert atm.); addn. of tert-butylpyridine to toluene soln. of zinc compd., stirring for 2 h; concg., keeping at -30°C for 24 h, isolation of crystals, elem. anal.;
DOI:10.1021/om1008549

Reference yield: 89.0%

: 1256380-63-8
[(tBuC(NDipp-κ1N)(η3-NDipp))ZnMe]

: 7553-56-2,12190-71-5,8031-47-8
iodine

: [((tBuC(NDipp)2-N,N')Zn(μ-I))2]

Guidance literature:: In toluene; byproducts: CH3I; (inert atm.); addn. of toluene soln. of iodine to toluene soln. of zinc compd. at -30°C, warming ot room temp., stirring for 12 h; filtration, recrystn. (toluene/diethyl ether) -30°C for 24 h, elem. anal.;
DOI:10.1021/om1008549