ethyl 2-phenylcyclohexeneacetate

Base Information

• Chemical Name: ethyl 2-phenylcyclohexeneacetate
• CAS No.: 170931-98-3
• Molecular Formula: C₁₆H₂₀O₂
• Molecular Weight: 244.334
• Mol file: 170931-98-3.mol

Synonyms:

Chemical Property of ethyl 2-phenylcyclohexeneacetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ethyl 2-phenylcyclohexeneacetate

There total 6 articles about ethyl 2-phenylcyclohexeneacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 1-hydroxy-2-phenylcyclohexaneacetate (170931-97-2) → ethyl 2-phenylcyclohexeneacetate (170931-98-3)

Guidance literature:

With pyridine; thionyl chloride; diethyl ether;

DOI:10.1039/jr9360000071

Reference yield:

(RS)-2-phenylcyclohexanone (1444-65-1) → ethyl 2-phenylcyclohexeneacetate (170931-98-3)

Guidance literature:

Multi-step reaction with 2 steps

1: zinc; benzene

2: thionyl chloride; diethyl ether; pyridine

With pyridine; thionyl chloride; diethyl ether; zinc; benzene;

DOI:10.1039/jr9360000071

Reference yield:

ethyl 1-hydroxy-2-phenylcyclohexaneacetate (170931-97-2) → ethyl 2-phenylcyclohexeneacetate (170931-98-3) + ethyl 2-phenylcyclohexylideneacetate (19909-99-0)

Guidance literature:

With pyridine; thionyl chloride; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.1016/0040-4020(95)00373-G

upstream raw materials:

ethyl 1-hydroxy-2-phenylcyclohexaneacetate

(RS)-2-phenylcyclohexanone

trimethylsilanyl-acetic acid ethyl ester

trans-2-Phenylcyclohexanol

Downstream raw materials:

trans-(2-phenylcyclohexyl)acetic acid

(+/-)-(cis-2-phenyl-cyclohexyl)-acetic acid

(2-phenyl-cyclohexyl)-acetic acid ethyl ester

(2-phenyl-cyclohex-1-enyl)-acetic acid