Technology Process of CNH2C7H7HC2H2C3N2H2C7H7
There total 6 articles about CNH2C7H7HC2H2C3N2H2C7H7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: molecular sieves 4 Angstroem / methanol / 3 h
2: NaBH4; MeOH / 5 h
With
methanol; sodium tetrahydroborate; 4 A molecular sieve;
In
methanol;
DOI:10.1021/jo0626008
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 98 percent / NaH / dimethylformamide / 0 - 40 °C
2: 80 percent / DIBAL-H / CH2Cl2; hexane / -78 - 20 °C
3: 96 percent / MnO2 / CH2Cl2 / 24 h / Heating
4: molecular sieves 4 Angstroem / methanol / 3 h
5: NaBH4; MeOH / 5 h
With
methanol; manganese(IV) oxide; sodium tetrahydroborate; 4 A molecular sieve; sodium hydride; diisobutylaluminium hydride;
In
methanol; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo0626008
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 98 percent / NaH / dimethylformamide / 0 - 40 °C
2: 80 percent / DIBAL-H / CH2Cl2; hexane / -78 - 20 °C
3: 96 percent / MnO2 / CH2Cl2 / 24 h / Heating
4: molecular sieves 4 Angstroem / methanol / 3 h
5: NaBH4; MeOH / 5 h
With
methanol; manganese(IV) oxide; sodium tetrahydroborate; 4 A molecular sieve; sodium hydride; diisobutylaluminium hydride;
In
methanol; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo0626008