3,22-bis(tert-butylsulfanyl)-28,29-dinitro-5,6,12,13,19,20,25,26,31,32-decadehydro-27,30-etheno-7,11:14,18-dimethenodibenzo[a,k]cyclooctacosane

Base Information

Chemical Name:3,22-bis(tert-butylsulfanyl)-28,29-dinitro-5,6,12,13,19,20,25,26,31,32-decadehydro-27,30-etheno-7,11:14,18-dimethenodibenzo[a,k]cyclooctacosane
CAS No.:914673-96-4
Molecular Formula:C₄₈H₃₄N₂O₄S₂
Molecular Weight:766.941
Hs Code.:

3,22-bis(tert-butylsulfanyl)-28,29-dinitro-5,6,12,13,19,20,25,26,31,32-decadehydro-27,30-etheno-7,11:14,18-dimethenodibenzo[a,k]cyclooctacosane

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Chemical Property of 3,22-bis(tert-butylsulfanyl)-28,29-dinitro-5,6,12,13,19,20,25,26,31,32-decadehydro-27,30-etheno-7,11:14,18-dimethenodibenzo[a,k]cyclooctacosane

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Technology Process of 3,22-bis(tert-butylsulfanyl)-28,29-dinitro-5,6,12,13,19,20,25,26,31,32-decadehydro-27,30-etheno-7,11:14,18-dimethenodibenzo[a,k]cyclooctacosane

There total 1 articles about 3,22-bis(tert-butylsulfanyl)-28,29-dinitro-5,6,12,13,19,20,25,26,31,32-decadehydro-27,30-etheno-7,11:14,18-dimethenodibenzo[a,k]cyclooctacosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 914673-85-1
1,4-diethynyl-2,3-dinitrobenzene

: 914673-89-5
3,3'-bis[(5-tert-butylsulfanyl-2-iodophenyl)ethynyl]tolane

: 914673-96-4
3,22-bis(tert-butylsulfanyl)-28,29-dinitro-5,6,12,13,19,20,25,26,31,32-decadehydro-27,30-etheno-7,11:14,18-dimethenodibenzo[a,k]cyclooctacosane

: 914673-95-3
3-{[5-tert-butylsulfanyl-3-(4'-ethynyl-2',3'-dinitrophenyl)ethynyl]phenylethynyl}-3'-(5-tert-butylsulfanyl-2-iodophenylethynyl)tolane

Guidance literature:: With copper(l) iodide; N-ethyl-N,N-diisopropylamine; triphenylphosphine; Pd(dibenzylideneacetone)2 chloroform adduct; In tetrahydrofuran;
DOI:10.1002/ejoc.200600336