1-(2-bromophenylmethyl)cyclopenta-1,3-diene

Base Information

Chemical Name:1-(2-bromophenylmethyl)cyclopenta-1,3-diene
CAS No.:114325-60-9
Molecular Formula:C₁₂H₁₁Br
Molecular Weight:235.123
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2-bromophenylmethyl)cyclopenta-1,3-diene

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Technology Process of 1-(2-bromophenylmethyl)cyclopenta-1,3-diene

There total 1 articles about 1-(2-bromophenylmethyl)cyclopenta-1,3-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: sodium cyclopentadienide

: 3433-80-5
1-Bromo-2-bromomethyl-benzene

: 114325-60-9
1-(2-bromophenylmethyl)cyclopenta-1,3-diene

: 2-(2-bromophenylmethyl)cyclopenta-1,3-diene

Guidance literature:: In ammonia; pentane; at -78 ℃; for 3h; Title compound not separated from byproducts;
DOI:10.1016/j.jorganchem.2003.08.045

Reference yield: 80.0%

: trichloro(η5-indenyl)zirconium

: 114325-60-9
1-(2-bromophenylmethyl)cyclopenta-1,3-diene

: 2-(2-bromophenylmethyl)cyclopenta-1,3-diene

: 654057-62-2
(η5:indenyl)(η5:C5H4-CH2C6H4-o-Br)2ZrCl2

Guidance literature:: With n-butyllithium; In diethyl ether; hexane; soln. of the cyclopentadiene derivative (isomeric mixt.) in Et2O treatedwith n-BuLi in n-hexane at -78°C; ZrCl3(indenyl) added at -78.de gree.C; mixt. stirred at room temp. overnight; concd. under vac.; suspn. filtered through Na2SO4; residue extd. with CH2Cl2; concd.; crystn. at -20°C;
DOI:10.1016/j.jorganchem.2003.08.045

Reference yield: 70.0%

: 10026-11-6
zirconium(IV) chloride

: 114325-60-9
1-(2-bromophenylmethyl)cyclopenta-1,3-diene

: 2-(2-bromophenylmethyl)cyclopenta-1,3-diene

: 654057-47-3
(η5:C5H4-CH2C6H4-o-Br)2ZrCl2

Guidance literature:: With n-butyllithium; In diethyl ether; hexane; soln. of the cyclopentadiene derivative (isomeric mixt.) in Et2O treatedwith n-BuLi in n-hexane at -78°C; ZrCl4 added at -78°C; m ixt. stirred at room temp. overnight; suspn. filtered through Na2SO4; soln. evapd. under vac.; residue washed twice with n-pentane and dried under vac.;
DOI:10.1016/j.jorganchem.2003.08.045