azido{bis(trimethylsilyl)amino}bis{(2,4,6-trimethylphenyl)(trimethylsiyl)amino}germane

Base Information

• Chemical Name: azido{bis(trimethylsilyl)amino}bis{(2,4,6-trimethylphenyl)(trimethylsiyl)amino}germane
• CAS No.: 117226-56-9
• Molecular Formula: C₃₀H₅₈GeN₆Si₄
• Molecular Weight: 687.763
• Mol file: 117226-56-9.mol

Synonyms:

Chemical Property of azido{bis(trimethylsilyl)amino}bis{(2,4,6-trimethylphenyl)(trimethylsiyl)amino}germane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of azido{bis(trimethylsilyl)amino}bis{(2,4,6-trimethylphenyl)(trimethylsiyl)amino}germane

There total 1 articles about azido{bis(trimethylsilyl)amino}bis{(2,4,6-trimethylphenyl)(trimethylsiyl)amino}germane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

bis{(2,4,6-trimethylphenyl)(trimethylsilyl)amino}germane(II) (97217-33-9) + trimethylsilylazide (4648-54-8) → azido{bis(trimethylsilyl)amino}bis{(2,4,6-trimethylphenyl)(trimethylsiyl)amino}germane (117226-56-9)

Guidance literature:

In tetrahydrofuran; byproducts: N2; to a soln. of Ge(N(Si(CH3)3)(2,4,6-(CH3)3C6H2))2 was added dropwise (CH3)3SiN3 at 20°C, after 12 h the soln. was filtered, solvent was removed under vac.; washed with THF; elem. anal.;

upstream raw materials:

bis{(2,4,6-trimethylphenyl)(trimethylsilyl)amino}germane(II)

trimethylsilylazide