1-(2-phenylethenyl)-3,3a,4,5-tetrahydroimidazo<1,5-a>quinoline

Base Information

Chemical Name:1-(2-phenylethenyl)-3,3a,4,5-tetrahydroimidazo<1,5-a>quinoline
CAS No.:128624-26-0
Molecular Formula:C₁₉H₁₈N₂
Molecular Weight:274.365
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2-phenylethenyl)-3,3a,4,5-tetrahydroimidazo<1,5-a>quinoline

Chemical Property:

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Technology Process of 1-(2-phenylethenyl)-3,3a,4,5-tetrahydroimidazo<1,5-a>quinoline

There total 5 articles about 1-(2-phenylethenyl)-3,3a,4,5-tetrahydroimidazo<1,5-a>quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5382-42-3
quinoline-2-carboxamide

: 128624-26-0
1-(2-phenylethenyl)-3,3a,4,5-tetrahydroimidazo<1,5-a>quinoline

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / hydrobromic acid, H₂ / aq. ethanol / 1 h / 22800 Torr / Heating; Adams catalyst

2: 1) diborane, 2) hydrochloric acid / 1) THF, 3d, reflux, 2) reflux, 1h

3: 52 percent / ethanol / 4.5 h / Heating

With hydrogenchloride; hydrogen bromide; hydrogen; diborane; In ethanol;

Reference yield:

: 1436-43-7
quinoline-2-carbonitrile

: 128624-26-0
1-(2-phenylethenyl)-3,3a,4,5-tetrahydroimidazo<1,5-a>quinoline

Guidance literature:: Multi-step reaction with 5 steps

1: 77 percent / 3percent hydrogen peroxide, 25percent potassium hydroxide / H₂O / 40 deg C, then 3h without heat

2: 70 percent / hydrobromic acid, H₂ / aq. ethanol / 1 h / 22800 Torr / Heating; Adams catalyst

3: 1) diborane, 2) hydrochloric acid / 1) THF, 3d, reflux, 2) reflux, 1h

4: 52 percent / ethanol / 4.5 h / Heating

With hydrogenchloride; potassium hydroxide; hydrogen bromide; hydrogen; dihydrogen peroxide; diborane; In ethanol; water;

Reference yield:

: 91842-88-5
1,2,3,4-tetrahydroquinoline-2-carboxamide

: 128624-26-0
1-(2-phenylethenyl)-3,3a,4,5-tetrahydroimidazo<1,5-a>quinoline

Guidance literature:: Multi-step reaction with 3 steps

1: 1) diborane, 2) hydrochloric acid / 1) THF, 3d, reflux, 2) reflux, 1h

2: 52 percent / ethanol / 4.5 h / Heating

With hydrogenchloride; diborane; In ethanol;