2-[(2S,3S,6R)-3-(3-Acetoxy-2-benzoylamino-propionylamino)-6-(5-acetoxymethyl-4-amino-2-oxo-2H-pyrimidin-1-yl)-3,6-dihydro-2H-pyran-2-yl]-2,4-dihydroxy-5-ureido-pentanoic acid

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Chemical Name:2-[(2S,3S,6R)-3-(3-Acetoxy-2-benzoylamino-propionylamino)-6-(5-acetoxymethyl-4-amino-2-oxo-2H-pyrimidin-1-yl)-3,6-dihydro-2H-pyran-2-yl]-2,4-dihydroxy-5-ureido-pentanoic acid
CAS No.:79190-07-1
Molecular Formula:C₃₀H₃₇N₇O₁₃
Molecular Weight:703.663
Hs Code.:

2-[(2S,3S,6R)-3-(3-Acetoxy-2-benzoylamino-propionylamino)-6-(5-acetoxymethyl-4-amino-2-oxo-2H-pyrimidin-1-yl)-3,6-dihydro-2H-pyran-2-yl]-2,4-dihydroxy-5-ureido-pentanoic acid

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Chemical Property of 2-[(2S,3S,6R)-3-(3-Acetoxy-2-benzoylamino-propionylamino)-6-(5-acetoxymethyl-4-amino-2-oxo-2H-pyrimidin-1-yl)-3,6-dihydro-2H-pyran-2-yl]-2,4-dihydroxy-5-ureido-pentanoic acid

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Technology Process of 2-[(2S,3S,6R)-3-(3-Acetoxy-2-benzoylamino-propionylamino)-6-(5-acetoxymethyl-4-amino-2-oxo-2H-pyrimidin-1-yl)-3,6-dihydro-2H-pyran-2-yl]-2,4-dihydroxy-5-ureido-pentanoic acid

There total 5 articles about 2-[(2S,3S,6R)-3-(3-Acetoxy-2-benzoylamino-propionylamino)-6-(5-acetoxymethyl-4-amino-2-oxo-2H-pyrimidin-1-yl)-3,6-dihydro-2H-pyran-2-yl]-2,4-dihydroxy-5-ureido-pentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67527-71-3
mildiomycin

: 79190-07-1
2-[(2S,3S,6R)-3-(3-Acetoxy-2-benzoylamino-propionylamino)-6-(5-acetoxymethyl-4-amino-2-oxo-2H-pyrimidin-1-yl)-3,6-dihydro-2H-pyran-2-yl]-2,4-dihydroxy-5-ureido-pentanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 11.2 g / 0.2 N NaOH / H₂O / 2 h / Heating

2: 4.4 g / 5percent NaHCO₃ / 3 h / 25 °C

3: 195 mg / acetic acid; pyridine / 3 h / 25 °C

With sodium hydroxide; sodium hydrogencarbonate; In pyridine; water; acetic acid;
DOI:10.1016/S0040-4020(01)92447-0

Reference yield:

: N-{1-[(2S,3S,6R)-6-(4-Amino-5-hydroxymethyl-2-oxo-2H-pyrimidin-1-yl)-2-(3-hydroxy-2-oxo-5-ureidomethyl-tetrahydro-furan-3-yl)-3,6-dihydro-2H-pyran-3-ylcarbamoyl]-2-hydroxy-ethyl}-benzamide

: 79190-07-1
2-[(2S,3S,6R)-3-(3-Acetoxy-2-benzoylamino-propionylamino)-6-(5-acetoxymethyl-4-amino-2-oxo-2H-pyrimidin-1-yl)-3,6-dihydro-2H-pyran-2-yl]-2,4-dihydroxy-5-ureido-pentanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 2percent NH₄OH / 4 h / 25 °C

2: 195 mg / acetic acid; pyridine / 3 h / 25 °C

With ammonium hydroxide; In pyridine; acetic acid;
DOI:10.1016/S0040-4020(01)92447-0

Reference yield:

: 67983-10-2
(2R,4R)-2-[(2S)-6c-(4-amino-5-hydroxymethyl-2-oxo-2H-pyrimidin-1-yl)-3t-L-serylamino-3,6-dihydro-2H-pyran-2r-yl]-5-ureido-2,4-dihydroxy-pentanoic acid

: 79190-07-1
2-[(2S,3S,6R)-3-(3-Acetoxy-2-benzoylamino-propionylamino)-6-(5-acetoxymethyl-4-amino-2-oxo-2H-pyrimidin-1-yl)-3,6-dihydro-2H-pyran-2-yl]-2,4-dihydroxy-5-ureido-pentanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 4.4 g / 5percent NaHCO₃ / 3 h / 25 °C

2: 195 mg / acetic acid; pyridine / 3 h / 25 °C

With sodium hydrogencarbonate; In pyridine; acetic acid;
DOI:10.1016/S0040-4020(01)92447-0