2-acetamido-1-phenylselenodecane

Base Information

• Chemical Name: 2-acetamido-1-phenylselenodecane
• CAS No.: 77037-10-6
• Molecular Formula: C₁₈H₂₉NOSe
• Molecular Weight: 354.394
• Mol file: 77037-10-6.mol

Synonyms:

Chemical Property of 2-acetamido-1-phenylselenodecane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-acetamido-1-phenylselenodecane

There total 2 articles about 2-acetamido-1-phenylselenodecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1-Decene (872-05-9,17438-89-0,25189-70-2) + diphenyl diselenide (1666-13-3) + acetonitrile (75-05-8,26809-02-9) → 2-acetamido-1-phenylselenodecane (77037-10-6)

Guidance literature:

With tetrabutylammonium tetrafluoroborate; electrolytic process;

DOI:10.1016/0040-4039(80)80190-0

Reference yield:

Phenylselenyl chloride (5707-04-0) + 1-Decene (872-05-9,17438-89-0,25189-70-2) + acetonitrile (75-05-8,26809-02-9) → 2-acetamido-1-phenylselenodecane (77037-10-6) + N-(2-Phenylselanyl-decyl)-acetamide (78837-71-5)

Guidance literature:

With trifluorormethanesulfonic acid; water; for 3h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Heating;

DOI:10.1021/jo00336a021

upstream raw materials:

Phenylselenyl chloride

1-Decene

acetonitrile

diphenyl diselenide

Refernces

• 1、 Bewick, Alan,Coe, David E.,Fuller, Geoffrey B.,Mellor, John M.. "Anodic acetamidoselenation of alkenes". . p. 3827 - 3828. Retrieved 2007/10/02.