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Technology Process of (C5H4Cl)(C6H6)Fe(1+)*PF6(1-) = [(C5H4Cl)(C6H6)Fe][PF6]

(C5H4Cl)(C6H6)Fe(1+)*PF6(1-) = [(C5H4Cl)(C6H6)Fe][PF6]

Base Information
  • Chemical Name:(C5H4Cl)(C6H6)Fe(1+)*PF6(1-) = [(C5H4Cl)(C6H6)Fe][PF6]
  • CAS No.:12282-28-9
  • Molecular Formula:C11H10ClFe*F6P
  • Molecular Weight:378.465
  • Hs Code.:
(C<sub>5</sub>H<sub>4</sub>Cl)(C<sub>6</sub>H<sub>6</sub>)Fe<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup> = [(C<sub>5</sub>H<sub>4</sub>Cl)(C<sub>6</sub>H<sub>6</sub>)Fe][PF<sub>6</sub>]

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Chemical Property of (C5H4Cl)(C6H6)Fe(1+)*PF6(1-) = [(C5H4Cl)(C6H6)Fe][PF6]
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Technology Process of (C5H4Cl)(C6H6)Fe(1+)*PF6(1-) = [(C5H4Cl)(C6H6)Fe][PF6]

There total 1 articles about (C5H4Cl)(C6H6)Fe(1+)*PF6(1-) = [(C5H4Cl)(C6H6)Fe][PF6] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

ammonium hexafluorophosphate

ammonium hexafluorophosphate

1,1’-dichloroferrocene
1293-67-0

1,1’-dichloroferrocene

ferrocenylbenzene

ferrocenylbenzene

(C<sub>5</sub>H<sub>4</sub>Cl)(C<sub>6</sub>H<sub>6</sub>)Fe<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup> = [(C<sub>5</sub>H<sub>4</sub>Cl)(C<sub>6</sub>H<sub>6</sub>)Fe][PF<sub>6</sub>]
12282-28-9

(C5H4Cl)(C6H6)Fe(1+)*PF6(1-) = [(C5H4Cl)(C6H6)Fe][PF6]

1,1'-diphenylferrocene

1,1'-diphenylferrocene

Guidance literature:
With aluminium trichloride; sodium thiosulfate; benzene; In benzene; byproducts: chloroferrocene, ferrocene; 2 equiv. AlCl3, heated to 100°C, stirred under N2 for 5 h, cooled, added with stirring to ice-cold water, Na2S2O3 soln. added, layers separated, aq. layer washed with ether and organic layer with H2O, saturated aq. NH4PF6 soln. added; salt pptd. (repptd. from acetone/ether or column chromy. on alumina with acetone/CH2Cl2, crystd. from MeOH), soln. dried (MgSO4), evapd., chromy. on alumina with light petroleum/CH2Cl2, rechromy. on silica, crystd. from MeOH or light petroleum;
upstream raw materials:

1,1’-dichloroferrocene

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