4-[N,N-di(4-tolyl)amino]benzaldehyde 4-methylbenzoylhydrazone

Base Information

• Chemical Name: 4-[N,N-di(4-tolyl)amino]benzaldehyde 4-methylbenzoylhydrazone
• CAS No.: 1612251-96-3
• Molecular Formula: C₂₉H₂₇N₃O
• Molecular Weight: 433.553
• Mol file: 1612251-96-3.mol

Synonyms:

Chemical Property of 4-[N,N-di(4-tolyl)amino]benzaldehyde 4-methylbenzoylhydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-[N,N-di(4-tolyl)amino]benzaldehyde 4-methylbenzoylhydrazone

There total 3 articles about 4-[N,N-di(4-tolyl)amino]benzaldehyde 4-methylbenzoylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-phenyl-di-p-tolylamine (20440-95-3) → 4-[N,N-di(4-tolyl)amino]benzaldehyde 4-methylbenzoylhydrazone (1612251-96-3)

Guidance literature:

Multi-step reaction with 2 steps

1: trichlorophosphate / 6 h / 25 - 130 °C

2: acetic acid / ethanol / 5 h / 70 °C

With acetic acid; trichlorophosphate; In ethanol; 1: |Vilsmeier-Haack Formylation;

DOI:10.1016/j.dyepig.2014.04.021

Reference yield:

di-p-tolylamine (620-93-9) → 4-[N,N-di(4-tolyl)amino]benzaldehyde 4-methylbenzoylhydrazone (1612251-96-3)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium hydroxide; copper(l) chloride; 1,10-Phenanthroline / water

2: trichlorophosphate / 6 h / 25 - 130 °C

3: acetic acid / ethanol / 5 h / 70 °C

With 1,10-Phenanthroline; acetic acid; copper(l) chloride; potassium hydroxide; trichlorophosphate; In ethanol; water; 1: |Ullmann Condensation / 2: |Vilsmeier-Haack Formylation;

DOI:10.1016/j.dyepig.2014.04.021

Reference yield:

iodobenzene (591-50-4) → 4-[N,N-di(4-tolyl)amino]benzaldehyde 4-methylbenzoylhydrazone (1612251-96-3)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium hydroxide; copper(l) chloride; 1,10-Phenanthroline / water

2: trichlorophosphate / 6 h / 25 - 130 °C

3: acetic acid / ethanol / 5 h / 70 °C

With 1,10-Phenanthroline; acetic acid; copper(l) chloride; potassium hydroxide; trichlorophosphate; In ethanol; water; 1: |Ullmann Condensation / 2: |Vilsmeier-Haack Formylation;

DOI:10.1016/j.dyepig.2014.04.021

upstream raw materials:

N-phenyl-di-p-tolylamine

iodobenzene

di-p-tolylamine