C₅H₃N(C₈H₄NC₄NO₂CH₂C₆H₅)RhCl₂(C₄H₈S)2

Base Information

Chemical Name:C₅H₃N(C₈H₄NC₄NO₂CH₂C₆H₅)RhCl₂(C₄H₈S)2
CAS No.:1369582-92-2
Molecular Formula:C₃₂H₃₀Cl₂N₃O₂RhS₂
Molecular Weight:726.553
Hs Code.:

C<sub>5</sub>H<sub>3</sub>N(C<sub>8</sub>H<sub>4</sub>NC<sub>4</sub>NO<sub>2</sub>CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)RhCl<sub>2</sub>(C<sub>4</sub>H<sub>8</sub>S)2

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Suppliers and Price of C₅H₃N(C₈H₄NC₄NO₂CH₂C₆H₅)RhCl₂(C₄H₈S)2

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Chemical Property of C₅H₃N(C₈H₄NC₄NO₂CH₂C₆H₅)RhCl₂(C₄H₈S)2

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Technology Process of C₅H₃N(C₈H₄NC₄NO₂CH₂C₆H₅)RhCl₂(C₄H₈S)2

There total 1 articles about C₅H₃N(C₈H₄NC₄NO₂CH₂C₆H₅)RhCl₂(C₄H₈S)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 35933-36-9,52611-16-2
RhCl₃(tetrahydrothiophen)3

: 1234890-16-4
C₆H₄C₂NH(C₅H₃N)C₄O₂N(benzyl)

: 1369582-92-2
C₅H₃N(C₈H₄NC₄NO₂CH₂C₆H₅)RhCl₂(C₄H₈S)2

Guidance literature:: In ethanol; water; suspn. in EtOH/H2O (1:) heated at reflux (90°C) for 16 h; cooled to room temp.; solvent evapd.; residue purified by silica gel chromy. with CH2Cl2/MeOH (100:1);
DOI:10.1002/ejic.201101175

Reference yield: 50.0%

: 1369582-92-2
C₅H₃N(C₈H₄NC₄NO₂CH₂C₆H₅)RhCl₂(C₄H₈S)2

: 4730-54-5
1,4,7-triazacyclononane

: C₅H₃N(C₈H₄NC₄NO₂CH₂C₆H₅)RhCl(CH₂CH₂NH)3⁽¹⁺⁾*NO₃^(1-)=[C₅H₃N(C₈H₄NC₄NO₂CH₂C₆H₅)RhCl(CH₂CH₂NH)3](NO₃)

Guidance literature:: In N,N-dimethyl-formamide; dissolved in DMF; stirred at 120°C for 16 h; solvent removed in vac; residue purified by silica gel chromy. with MeCN/aq. KNO3; solvent of eluent removed; residue dissolved in MeCN/water; pptd. with excess water; solid isolated by centrifugation; washed with water, dried in vac.;
DOI:10.1002/ejic.201101175

Reference yield: 41.0%

: 6573-11-1
1,4,7-trithiacyclononane

: 1369582-92-2
C₅H₃N(C₈H₄NC₄NO₂CH₂C₆H₅)RhCl₂(C₄H₈S)2

: C₅H₃N(C₈H₄NC₄NO₂CH₂C₆H₅)RhCl(CH₂CH₂S)3⁽¹⁺⁾*NO₃^(1-)=[C₅H₃N(C₈H₄NC₄NO₂CH₂C₆H₅)RhCl(CH₂CH₂S)3](NO₃)

Guidance literature:: In N,N-dimethyl-formamide; dissolved in DMF; stirred at 120°C for 16 h; solvent removed in vac; residue purified by silica gel chromy. with MeCN/aq. KNO3; solvent of eluent removed; residue dissolved in MeCN/water; pptd. with excess water; solid isolated by centrifugation; washed with water, dried in vac.;
DOI:10.1002/ejic.201101175