RhCl(CO)[(C₆H₅)2N(PO₂C₃H₆)]2

Base Information

Chemical Name:RhCl(CO)[(C₆H₅)2N(PO₂C₃H₆)]2
CAS No.:81953-67-5
Molecular Formula:C₃₁H₃₂ClN₂O₅P₂Rh
Molecular Weight:712.911
Hs Code.:

RhCl(CO)[(C<sub>6</sub>H<sub>5</sub>)2N(PO<sub>2</sub>C<sub>3</sub>H<sub>6</sub>)]2

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Chemical Property of RhCl(CO)[(C₆H₅)2N(PO₂C₃H₆)]2

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Technology Process of RhCl(CO)[(C₆H₅)2N(PO₂C₃H₆)]2

There total 3 articles about RhCl(CO)[(C₆H₅)2N(PO₂C₃H₆)]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: tetracarbonyldi-μ-chlorodirhodium(I)

: 60197-03-7
2-(diphenylamino)-1,3,2-dioxaphosphorinane

: 81953-67-5,82838-13-9
RhCl(CO)[(C₆H₅)2N(PO₂C₃H₆)]2

Guidance literature:: In diethyl ether; (N2); (C6H5)2N(PO2C3H6) in ether ia added with stirring to (RhCl(CO)2)2in ether; evapn. in vacuo at 20°C; chromy. (silica gel, benzene, benzene/dioxane); evapn. in vacuo at 20°C, (dry inert gas); pptd. (hexane)at liq. nitrogen temp.; elem. anal., MS anal.;

Reference yield: 77.0%

: 17454-25-0
2-(dimethylamino)-1,3,2-dioxaphosphorinane

: 60197-03-7
2-(diphenylamino)-1,3,2-dioxaphosphorinane

: 81953-67-5,82838-13-9
RhCl(CO)[(C₆H₅)2N(PO₂C₃H₆)]2

Guidance literature:: In diethyl ether; byproducts: CO; org. ligand soln. addn. to Rh-complex soln. (vigorous stirring); ether removal (reduced pressure, 20°C, nitrogen atmosphere), repptn. (hexane); elem. anal.;

Reference yield:

: tetracarbonyldi-μ-chlorodirhodium(I)

: 60197-03-7
2-(diphenylamino)-1,3,2-dioxaphosphorinane

: 81953-67-5,82838-13-9
RhCl(CO)[(C₆H₅)2N(PO₂C₃H₆)]2

: 99193-08-5
[RhCl(CO)((C₆H₅)2N(PO₂C₃H₆))]2

Guidance literature:: In diethyl ether; byproducts: ((C6H5)2N)PO(O2C3H6); in air; the phosphorinane in ether is added with stirring to (RhCl(CO)2)2 in ether; evapn. in vacuo at 20°C; chromy. (silica gel, benzene, benzene/dioxane); evapn. in vacuo at 20°C, (dry inert gas); pptd. (hexane)at liq. nitrogen temp.;