dihydridobis(triphenylphosphine)(1,2-di(isopropylimino)ethane)ruthenium(II)

Base Information

Chemical Name:dihydridobis(triphenylphosphine)(1,2-di(isopropylimino)ethane)ruthenium(II)
CAS No.:71660-53-2
Molecular Formula:C₄₄H₄₈N₂P₂Ru
Molecular Weight:767.896
Hs Code.:

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Chemical Property of dihydridobis(triphenylphosphine)(1,2-di(isopropylimino)ethane)ruthenium(II)

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Technology Process of dihydridobis(triphenylphosphine)(1,2-di(isopropylimino)ethane)ruthenium(II)

There total 2 articles about dihydridobis(triphenylphosphine)(1,2-di(isopropylimino)ethane)ruthenium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: RuH₂(P(C₆H₅)3)4

: 28227-41-0,24764-90-7
1,4-diisopropyl-1,4-diazabuta-1,3-diene

: 71660-53-2,77210-59-4
dihydridobis(triphenylphosphine)(1,2-di(isopropylimino)ethane)ruthenium(II)

Guidance literature:: In toluene; under Ar, RuH2(PPh3)4 stirred in soln. of diazadiene in toluene for 2 d; concd., filtered, layered with hexane at room temp., crystals collected, washed with light petroleum, dried in vac.; elem. anal.;
DOI:10.1016/S0022-328X(00)82478-X

Reference yield: 15.0%

: 71770-10-0
chloro[1,2-di(isopropylimino)ethane]hydridobis(triphenylphosphine)ruthenium(II)

: 25360-32-1,22337-78-6
carbonyl bis(hydrido)tris(triphenylphosphine)ruthenium(II)

: 71660-53-2,77210-59-4
[RuH₂(P(C₆H₅)3)2(C₃H₇NCHCHNC₃H₇)]

: 71660-50-9
[Ru₂Cl₃(P(C₆H₅)3)2(C₃H₇NCHCHNC₃H₇)2]⁽¹⁺⁾

Guidance literature:: With methanol; In methanol; under N2 or Ar, 50°C, overnight; evapd., ppt. recrystd. from toluene/petropleum gave RuH2(PPh3)2(dad-a) and RuH2(CO)(PPh3)3; sol. evapd. to dryness, the oil crystd. from CH2Cl2/ether gave Ru2Cl3(PPh3)2(dad-a)2(1+);
DOI:10.1039/DT9800000539