3α-methoxyfriedelan

Base Information

• Chemical Name: 3α-methoxyfriedelan
• CAS No.: 87638-69-5
• Molecular Formula: C₃₁H₅₄O
• Molecular Weight: 442.769
• Mol file: 87638-69-5.mol

Synonyms:

Chemical Property of 3α-methoxyfriedelan

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3α-methoxyfriedelan

There total 2 articles about 3α-methoxyfriedelan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

friedelinol (7506-18-5,16844-71-6,105370-95-4,5085-72-3) + methyl iodide (74-88-4) → 3α-methoxyfriedelan (6939-65-7,87638-69-5)

Guidance literature:

With silver(l) oxide;

DOI:10.1021/ja01300a053

Reference yield:

friedelin (559-74-0) → 3α-methoxyfriedelan (6939-65-7,87638-69-5)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium; pentanol-⁽¹⁾

2: Ag₂O

With pentan-1-ol; sodium; silver(l) oxide;

DOI:10.1021/ja01300a053

Reference yield:

3α-methoxyfriedelan (6939-65-7,87638-69-5) → friedelinol (7506-18-5,16844-71-6,105370-95-4,5085-72-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 105 mg / PhOH, 47percent HBr / CHCl₃ / 7 h / Heating

2: 35 mg / 10percent methanolic KOH / methanol / 6 h / Heating

With potassium hydroxide; hydrogen bromide; phenol; In methanol; chloroform;

DOI:10.1016/0031-9422(83)83047-7

upstream raw materials:

friedelinol

methyl iodide

friedelin

Downstream raw materials:

friedelinol