8,20,31-Trioxa-5,11,14,17,23,28,34-heptaaza-tricyclo[12.12.10.1^3,25]heptatriaconta-1⁽²⁶⁾,2,25⁽³⁷⁾-triene; compound with toluene-4-sulfonic acid

Base Information

• Chemical Name: 8,20,31-Trioxa-5,11,14,17,23,28,34-heptaaza-tricyclo[12.12.10.1^3,25]heptatriaconta-1⁽²⁶⁾,2,25⁽³⁷⁾-triene; compound with toluene-4-sulfonic acid
• CAS No.: 109774-87-0
• Molecular Formula: 6C₇H₈O₃S*C₂₇H₅₁N₇O₃
• Molecular Weight: 1554.98

Synonyms:

Chemical Property of 8,20,31-Trioxa-5,11,14,17,23,28,34-heptaaza-tricyclo[12.12.10.1^3,25]heptatriaconta-1⁽²⁶⁾,2,25⁽³⁷⁾-triene; compound with toluene-4-sulfonic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 8,20,31-Trioxa-5,11,14,17,23,28,34-heptaaza-tricyclo[12.12.10.1^3,25]heptatriaconta-1⁽²⁶⁾,2,25⁽³⁷⁾-triene; compound with toluene-4-sulfonic acid

There total 6 articles about 8,20,31-Trioxa-5,11,14,17,23,28,34-heptaaza-tricyclo[12.12.10.1^3,25]heptatriaconta-1⁽²⁶⁾,2,25⁽³⁷⁾-triene; compound with toluene-4-sulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3,5-Tris(bromomethyl)benzene (18226-42-1) → 8,20,31-Trioxa-5,11,14,17,23,28,34-heptaaza-tricyclo[12.12.10.13,25]heptatriaconta-1(26),2,25(37)-triene; compound with toluene-4-sulfonic acid (109774-87-0)

Guidance literature:

Multi-step reaction with 6 steps

1: sodium azide

2: LiAlH₄

4: 48 percent / Cs₂CO₃ / dimethylformamide / 7 h / 80 °C

5: 33percent HBr, phenol / acetic acid / 24 h / 40 °C

6: ion exchange resin (basic form)

With lithium aluminium tetrahydride; sodium azide; ion exchange resin (basic form); hydrogen bromide; caesium carbonate; phenol; In acetic acid; N,N-dimethyl-formamide;

DOI:10.1016/S0040-4039(00)85349-6

Reference yield:

1,3,5-tris(aminomethyl)benzene (77372-56-6) → 8,20,31-Trioxa-5,11,14,17,23,28,34-heptaaza-tricyclo[12.12.10.13,25]heptatriaconta-1(26),2,25(37)-triene; compound with toluene-4-sulfonic acid (109774-87-0)

Guidance literature:

Multi-step reaction with 4 steps

2: 48 percent / Cs₂CO₃ / dimethylformamide / 7 h / 80 °C

3: 33percent HBr, phenol / acetic acid / 24 h / 40 °C

4: ion exchange resin (basic form)

With ion exchange resin (basic form); hydrogen bromide; caesium carbonate; phenol; In acetic acid; N,N-dimethyl-formamide;

DOI:10.1016/S0040-4039(00)85349-6

Reference yield:

1,3,5-tris(azidomethyl)benzene (107864-71-1) → 8,20,31-Trioxa-5,11,14,17,23,28,34-heptaaza-tricyclo[12.12.10.13,25]heptatriaconta-1(26),2,25(37)-triene; compound with toluene-4-sulfonic acid (109774-87-0)

Guidance literature:

Multi-step reaction with 5 steps

1: LiAlH₄

3: 48 percent / Cs₂CO₃ / dimethylformamide / 7 h / 80 °C

4: 33percent HBr, phenol / acetic acid / 24 h / 40 °C

5: ion exchange resin (basic form)

With lithium aluminium tetrahydride; ion exchange resin (basic form); hydrogen bromide; caesium carbonate; phenol; In acetic acid; N,N-dimethyl-formamide;

DOI:10.1016/S0040-4039(00)85349-6

upstream raw materials:

8,20,31-Trioxa-5,11,14,17,23,28,34-heptaaza-tricyclo[12.12.10.1^3,25]heptatriaconta-1⁽²⁶⁾,2,25⁽³⁷⁾-triene; hydrobromide

1,3,5-Tris(bromomethyl)benzene

1,3,5-tris(aminomethyl)benzene

1,3,5-tris(azidomethyl)benzene

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