N,N'-6,6'-tetramethyl,N,N'-(3-nitrophen-4,1-ylene)methylene(2-nitrophen-4,1-ylene)>>bis

Base Information

Chemical Name:N,N'-6,6'-tetramethyl,N,N'-(3-nitrophen-4,1-ylene)methylene(2-nitrophen-4,1-ylene)>>bis
CAS No.:156818-72-3
Molecular Formula:C₅₁H₄₃N₁₁O₁₂
Molecular Weight:1001.97
Hs Code.:

N,N'-6,6'-tetramethyl,N,N'-<pyridine-2,6-diylbis<<carbonyl(methyl)nitrilo>(3-nitrophen-4,1-ylene)methylene(2-nitrophen-4,1-ylene)>>bis<pyridine-2carboxamide>

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Chemical Property of N,N'-6,6'-tetramethyl,N,N'-(3-nitrophen-4,1-ylene)methylene(2-nitrophen-4,1-ylene)>>bis

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Technology Process of N,N'-6,6'-tetramethyl,N,N'-(3-nitrophen-4,1-ylene)methylene(2-nitrophen-4,1-ylene)>>bis

There total 3 articles about N,N'-6,6'-tetramethyl,N,N'-(3-nitrophen-4,1-ylene)methylene(2-nitrophen-4,1-ylene)>>bis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 3739-94-4
2,6-Pyridinedicarbonyl dichloride

: 156818-62-1
N,6-dimethyl-N-<4'-<4''-(methylamino)-3''-nitrobenzyl>-2'-nitrophenyl>pyridine-2-carboxamide

: 156818-72-3
N,N'-6,6'-tetramethyl,N,N'-(3-nitrophen-4,1-ylene)methylene(2-nitrophen-4,1-ylene)>>bis

Guidance literature:: With triethylamine; In dichloromethane; for 21h; Heating;
DOI:10.1002/hlca.19940770406

Reference yield:

: 934-60-1
6-methyl-2-pyridinecarboxylic acid

: 156818-72-3
N,N'-6,6'-tetramethyl,N,N'-(3-nitrophen-4,1-ylene)methylene(2-nitrophen-4,1-ylene)>>bis

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / dimethylformamide / 1.5 h / Heating

2: 50 percent / Et₃N / CHCl₃ / 15 h / Ambient temperature

3: 73 percent / Et₃N / CH₂Cl₂ / 21 h / Heating

With thionyl chloride; triethylamine; In dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19940770406

Reference yield:

: 126125-54-0
6-methyl-pyridine-2-carbonyl chloride

: 156818-72-3
N,N'-6,6'-tetramethyl,N,N'-(3-nitrophen-4,1-ylene)methylene(2-nitrophen-4,1-ylene)>>bis

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / Et₃N / CHCl₃ / 15 h / Ambient temperature

2: 73 percent / Et₃N / CH₂Cl₂ / 21 h / Heating

With triethylamine; In dichloromethane; chloroform;
DOI:10.1002/hlca.19940770406