1,1'-bis(diphenylphosphino)cobaltocenium nitrate

Base Information

Chemical Name:1,1'-bis(diphenylphosphino)cobaltocenium nitrate
CAS No.:222029-19-8
Molecular Formula:C₃₄H₂₈CoP₂*NO₃
Molecular Weight:619.542
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Chemical Property of 1,1'-bis(diphenylphosphino)cobaltocenium nitrate

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Technology Process of 1,1'-bis(diphenylphosphino)cobaltocenium nitrate

There total 1 articles about 1,1'-bis(diphenylphosphino)cobaltocenium nitrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 67292-47-1
1,1'-bis(diphenylphosphino)cobaltocene

: 7697-37-2,78989-43-2
nitric acid

: 222029-19-8
1,1'-bis(diphenylphosphino)cobaltocenium nitrate

Guidance literature:: In water; propionic acid anhydride; under N2 atm. to suspn. bis(diphenylphosphino)cobaltocene in propionic anhydride was added concd. nitric acid; soln. was added dropwise to ether, oil formed was washed with ether, dissolved in CH2Cl2 and added dropwise to ether, ppt. was filtered, washedwith ether, and dried in vacuo; elem. anal.;
DOI:10.1021/om000183y