C₁₂H₁₃NO₂

Base Information

Chemical Name:C₁₂H₁₃NO₂
CAS No.:1350810-05-7
Molecular Formula:C₁₂H₁₃NO₂
Molecular Weight:203.241
Hs Code.:

C<sub>12</sub>H<sub>13</sub>NO<sub>2</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₁₃NO₂

Chemical Property:

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Technology Process of C₁₂H₁₃NO₂

There total 5 articles about C₁₂H₁₃NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 1350809-94-7
C₁₂H₁₄INO₂

: 1350810-05-7
C₁₂H₁₃NO₂

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; silver(l) oxide; In toluene; at 120 ℃; for 24h; optical yield given as %de; Inert atmosphere;
DOI:10.1039/c1cc15257b

Reference yield:

: C₁₅H₂₁IO₃

: 1350810-05-7
C₁₂H₁₃NO₂

Guidance literature:: Multi-step reaction with 3 steps

1: water; toluene-4-sulfonic acid / acetone / 80 °C

2: ethanol / 6 h / 20 °C

3: bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; silver(l) oxide / toluene / 24 h / 120 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; water; potassium carbonate; toluene-4-sulfonic acid; silver(l) oxide; In ethanol; acetone; toluene; 3: Heck type reaction;
DOI:10.1039/c1cc15257b

Reference yield:

: 1350810-32-0
C₁₁H₁₁IO₂

: 1350810-05-7
C₁₂H₁₃NO₂

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 6 h / 20 °C

2: bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; silver(l) oxide / toluene / 24 h / 120 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; silver(l) oxide; In ethanol; toluene; 2: Heck type reaction;
DOI:10.1039/c1cc15257b