(R)-2-{(2R,3R)-2-[(2R,3R)-1-((R)-1-Carboxy-2-methyl-propyl)-4-oxo-3-phenylacetylamino-azetidin-2-yldisulfanyl]-4-oxo-3-phenylacetylamino-azetidin-1-yl}-3-methyl-butyric acid

Base Information

Chemical Name:(R)-2-{(2R,3R)-2-[(2R,3R)-1-((R)-1-Carboxy-2-methyl-propyl)-4-oxo-3-phenylacetylamino-azetidin-2-yldisulfanyl]-4-oxo-3-phenylacetylamino-azetidin-1-yl}-3-methyl-butyric acid
CAS No.:130164-51-1
Molecular Formula:C₃₂H₃₈N₄O₈S₂
Molecular Weight:670.808
Hs Code.:

(R)-2-{(2R,3R)-2-[(2R,3R)-1-((R)-1-Carboxy-2-methyl-propyl)-4-oxo-3-phenylacetylamino-azetidin-2-yldisulfanyl]-4-oxo-3-phenylacetylamino-azetidin-1-yl}-3-methyl-butyric acid

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Chemical Property of (R)-2-{(2R,3R)-2-[(2R,3R)-1-((R)-1-Carboxy-2-methyl-propyl)-4-oxo-3-phenylacetylamino-azetidin-2-yldisulfanyl]-4-oxo-3-phenylacetylamino-azetidin-1-yl}-3-methyl-butyric acid

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Technology Process of (R)-2-{(2R,3R)-2-[(2R,3R)-1-((R)-1-Carboxy-2-methyl-propyl)-4-oxo-3-phenylacetylamino-azetidin-2-yldisulfanyl]-4-oxo-3-phenylacetylamino-azetidin-1-yl}-3-methyl-butyric acid

There total 5 articles about (R)-2-{(2R,3R)-2-[(2R,3R)-1-((R)-1-Carboxy-2-methyl-propyl)-4-oxo-3-phenylacetylamino-azetidin-2-yldisulfanyl]-4-oxo-3-phenylacetylamino-azetidin-1-yl}-3-methyl-butyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 119944-09-1
(R)-2-((1R,5R)-3-Benzyl-7-oxo-4-thia-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-3-methyl-but-3-enoic acid benzhydryl ester

: 130164-51-1
(R)-2-{(2R,3R)-2-[(2R,3R)-1-((R)-1-Carboxy-2-methyl-propyl)-4-oxo-3-phenylacetylamino-azetidin-2-yldisulfanyl]-4-oxo-3-phenylacetylamino-azetidin-1-yl}-3-methyl-butyric acid

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / H₂ / (Ph₃P)3RhCl / benzene; ethanol / 11 h / 1034.3 Torr / Ambient temperature

2: 0.17 g / I₂, 1N HCl / dimethylsulfoxide / 3 h / Ambient temperature

3: 70 mg / TFA, anisole / 2 h

With hydrogenchloride; hydrogen; iodine; methoxybenzene; trifluoroacetic acid; Wilkinson's catalyst; In ethanol; dimethyl sulfoxide; benzene;

Reference yield:

: 51446-87-8
diphenylmethyl 6β-(2-phenylacetamido)penicillanate 1-oxide

: 130164-51-1
(R)-2-{(2R,3R)-2-[(2R,3R)-1-((R)-1-Carboxy-2-methyl-propyl)-4-oxo-3-phenylacetylamino-azetidin-2-yldisulfanyl]-4-oxo-3-phenylacetylamino-azetidin-1-yl}-3-methyl-butyric acid

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / P(OMe)3 / benzene / 40 h / Heating

2: 91 percent / H₂ / (Ph₃P)3RhCl / benzene; ethanol / 11 h / 1034.3 Torr / Ambient temperature

3: 0.17 g / I₂, 1N HCl / dimethylsulfoxide / 3 h / Ambient temperature

4: 70 mg / TFA, anisole / 2 h

With hydrogenchloride; hydrogen; iodine; methoxybenzene; trifluoroacetic acid; phosphorous acid trimethyl ester; Wilkinson's catalyst; In ethanol; dimethyl sulfoxide; benzene;

Reference yield:

: 4052-54-4
Penicillin G 1-(s)-oxide

: 130164-51-1
(R)-2-{(2R,3R)-2-[(2R,3R)-1-((R)-1-Carboxy-2-methyl-propyl)-4-oxo-3-phenylacetylamino-azetidin-2-yldisulfanyl]-4-oxo-3-phenylacetylamino-azetidin-1-yl}-3-methyl-butyric acid

Guidance literature:: Multi-step reaction with 5 steps

1: 96 percent / acetone

2: 80 percent / P(OMe)3 / benzene / 40 h / Heating

3: 91 percent / H₂ / (Ph₃P)3RhCl / benzene; ethanol / 11 h / 1034.3 Torr / Ambient temperature

4: 0.17 g / I₂, 1N HCl / dimethylsulfoxide / 3 h / Ambient temperature

5: 70 mg / TFA, anisole / 2 h

With hydrogenchloride; hydrogen; iodine; methoxybenzene; trifluoroacetic acid; phosphorous acid trimethyl ester; Wilkinson's catalyst; In ethanol; dimethyl sulfoxide; acetone; benzene;