1-benzyl-4-<2--N-methylamino>ethyl>piperidine

Base Information

Chemical Name:1-benzyl-4-<2--N-methylamino>ethyl>piperidine
CAS No.:126849-12-5
Molecular Formula:C₂₉H₃₄N₂O₃S
Molecular Weight:490.667
Hs Code.:

1-benzyl-4-<2-<N-<4'-(benzylsulfonyl)benzoyl>-N-methylamino>ethyl>piperidine

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-benzyl-4-<2--N-methylamino>ethyl>piperidine

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Technology Process of 1-benzyl-4-<2--N-methylamino>ethyl>piperidine

There total 9 articles about 1-benzyl-4-<2--N-methylamino>ethyl>piperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53136-21-3
1-benzylsulphanyl-4-bromobenzene

: 126849-12-5
1-benzyl-4-<2--N-methylamino>ethyl>piperidine

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) Mg, BrCH₂CH₂Br / 1.) THF, reflux, 1 h, 2.) 3 h

2: 87 percent / 33percent H₂O₂ / acetic acid / 1.5 h / 70 °C

3: 87 percent / SOCl₂ / 2 h / Heating

4: Et₃N / tetrahydrofuran / 0.67 h / Heating

5: NaOH / dimethylformamide / Ambient temperature

With sodium hydroxide; thionyl chloride; dihydrogen peroxide; magnesium; ethylene dibromide; triethylamine; In tetrahydrofuran; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jm00169a008

Reference yield:

: 70793-11-2
p-(benzylsulfonyl)benzoic acid

: 126849-12-5
1-benzyl-4-<2--N-methylamino>ethyl>piperidine

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / SOCl₂ / 2 h / Heating

2: Et₃N / tetrahydrofuran / 0.67 h / Heating

3: NaOH / dimethylformamide / Ambient temperature

With sodium hydroxide; thionyl chloride; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm00169a008

Reference yield:

: 22855-95-4
4-benzylsulfanylbenzoic acid

: 126849-12-5
1-benzyl-4-<2--N-methylamino>ethyl>piperidine

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / 33percent H₂O₂ / acetic acid / 1.5 h / 70 °C

2: 87 percent / SOCl₂ / 2 h / Heating

3: Et₃N / tetrahydrofuran / 0.67 h / Heating

4: NaOH / dimethylformamide / Ambient temperature

With sodium hydroxide; thionyl chloride; dihydrogen peroxide; triethylamine; In tetrahydrofuran; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jm00169a008